ST₀₃₃₀₆₁

Base Information

• Chemical Name: ST₀₃₃₀₆₁
• CAS No.: 416882-61-6
• Molecular Formula: C₁₅H₁₃FN₂O₂
• Molecular Weight: 272.279
• Mol file: 416882-61-6.mol

Synonyms:ST₀₃₃₀₆₁

Chemical Property of ST₀₃₃₀₆₁

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of ST₀₃₃₀₆₁

There total 3 articles about ST₀₃₃₀₆₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-fluorobezohydrazide (446-24-2) + o-hydroxyacetophenone (118-93-4,104809-67-8) → ST033061 (416882-61-6)

Guidance literature:

In ethanol; Reflux;

DOI:10.1016/j.tet.2014.01.059

Reference yield:

2-fluoro-benzoic acid ethyl ester (443-26-5) → ST033061 (416882-61-6)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrazine hydrate / 80 °C

2: ethanol / Reflux

With hydrazine hydrate; In ethanol;

DOI:10.1016/j.tet.2014.01.059

Reference yield:

o-fluoro-benzoic acid (445-29-4) → ST033061 (416882-61-6)

Guidance literature:

Multi-step reaction with 3 steps

1: thionyl chloride / 20 °C / Reflux

2: hydrazine hydrate / 80 °C

3: ethanol / Reflux

With thionyl chloride; hydrazine hydrate; In ethanol;

DOI:10.1016/j.tet.2014.01.059

upstream raw materials:

2-fluorobezohydrazide

o-hydroxyacetophenone

2-fluoro-benzoic acid ethyl ester

o-fluoro-benzoic acid

Downstream raw materials:

C₁₅H₁₁FO₂