2-amino-4-chloro-6-deuteronitrobenzene

Base Information

Chemical Name:2-amino-4-chloro-6-deuteronitrobenzene
CAS No.:353491-33-5
Molecular Formula:C₆H₅ClN₂O₂
Molecular Weight:173.563
Hs Code.:

Synonyms:2-amino-4-chloro-6-deuteronitrobenzene

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Chemical Property of 2-amino-4-chloro-6-deuteronitrobenzene

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Technology Process of 2-amino-4-chloro-6-deuteronitrobenzene

There total 3 articles about 2-amino-4-chloro-6-deuteronitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 353491-30-2
4-chloro-2,6-dideuteronitrobenzene

: 353491-33-5
2-amino-4-chloro-6-deuteronitrobenzene

Guidance literature:: With potassium tert-butylate; N,N,N-trimethylhydrazinium iodide; In dimethyl sulfoxide; N,N-dimethyl-formamide; at -40 ℃; for 0.216667h;
DOI:10.1016/S0040-4020(01)00398-2

Reference yield:

: 35749-94-1
4-chloro-2,6-dideuteroaniline

: 353491-33-5
2-amino-4-chloro-6-deuteronitrobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 59 percent / Oxone; NaHCO₃ / hexane; H₂O; acetone / 1 h / 0 °C

2: 64 percent / NH₂NMe₃⁽¹⁺⁾*I^(1-); t-BuOK / dimethylsulfoxide; dimethylformamide / 0.22 h / -40 °C

With Oxone; potassium tert-butylate; N,N,N-trimethylhydrazinium iodide; sodium hydrogencarbonate; In hexane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetone;
DOI:10.1016/S0040-4020(01)00398-2

Reference yield:

: 106-47-8
4-chloro-aniline

: 353491-33-5
2-amino-4-chloro-6-deuteronitrobenzene

Guidance literature:: Multi-step reaction with 3 steps

1: SOCl₂; D₂O / Heating

2: 59 percent / Oxone; NaHCO₃ / hexane; H₂O; acetone / 1 h / 0 °C

3: 64 percent / NH₂NMe₃⁽¹⁺⁾*I^(1-); t-BuOK / dimethylsulfoxide; dimethylformamide / 0.22 h / -40 °C

With Oxone; thionyl chloride; potassium tert-butylate; water-d2; N,N,N-trimethylhydrazinium iodide; sodium hydrogencarbonate; In hexane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetone;
DOI:10.1016/S0040-4020(01)00398-2