(1R,2R,6S)-2-methoxy-6-[(R)-(p-tolyl)sulfinyl]-3-cyclohexene-1-carbonitrile

Base Information

Chemical Name:(1R,2R,6S)-2-methoxy-6-[(R)-(p-tolyl)sulfinyl]-3-cyclohexene-1-carbonitrile
CAS No.:314777-38-3
Molecular Formula:C₁₅H₁₇NO₂S
Molecular Weight:275.371
Hs Code.:

Synonyms:(1R,2R,6S)-2-methoxy-6-[(R)-(p-tolyl)sulfinyl]-3-cyclohexene-1-carbonitrile

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Chemical Property of (1R,2R,6S)-2-methoxy-6-[(R)-(p-tolyl)sulfinyl]-3-cyclohexene-1-carbonitrile

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Technology Process of (1R,2R,6S)-2-methoxy-6-[(R)-(p-tolyl)sulfinyl]-3-cyclohexene-1-carbonitrile

There total 2 articles about (1R,2R,6S)-2-methoxy-6-[(R)-(p-tolyl)sulfinyl]-3-cyclohexene-1-carbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 10034-09-0
1-methoxy-1,3-butadiene

: 205251-17-8
(Z)-3-[(R)-p-tolylsulfinyl]propenonitrile

: 314777-38-3
(1R,2R,6S)-2-methoxy-6-[(R)-(p-tolyl)sulfinyl]-3-cyclohexene-1-carbonitrile

: (1R,2S,6S)-2-methoxy-6-[(R)-p-tolylsulfinyl]-3-cyclohexene-1-carbonitrile

Guidance literature:: In dichloromethane; at 20 ℃; for 96h;
DOI:10.1021/jo000963g

Reference yield: 13.0%

: 10034-09-0
1-methoxy-1,3-butadiene

: 205251-17-8
(Z)-3-[(R)-p-tolylsulfinyl]propenonitrile

: 314777-38-3
(1R,2R,6S)-2-methoxy-6-[(R)-(p-tolyl)sulfinyl]-3-cyclohexene-1-carbonitrile

: (1R,2S,6S)-2-methoxy-6-[(R)-p-tolylsulfinyl]-3-cyclohexene-1-carbonitrile

: (1S,2S,6R)-2-methoxy-6-[(R)-p-tolylsulfinyl]-3-cyclohexene-1-carbonitrile

Guidance literature:: With zinc dibromide; In dichloromethane; at 20 ℃; for 72h; under 3000300 Torr;
DOI:10.1021/jo000963g

Reference yield:

: 314777-38-3
(1R,2R,6S)-2-methoxy-6-[(R)-(p-tolyl)sulfinyl]-3-cyclohexene-1-carbonitrile

: (1S,2R,6S)-2-methoxy-6-[(p-tolyl)sulfenyl]-3-cyclohex-3-ene-1-carboxamide

Guidance literature:: (1R,2R,6S)-2-methoxy-6-[(R)-(p-tolyl)sulfinyl]-3-cyclohexene-1-carbonitrile; With boron trifluoride diethyl etherate; In dichloromethane; for 1h; Heating;

With sodium iodide; In dichloromethane; at 20 ℃; Further stages.;
DOI:10.1021/jo016174w