2,4-Dimethoxybenzohydroximinoyl chloride

Base Information

• Chemical Name: 2,4-Dimethoxybenzohydroximinoyl chloride
• CAS No.: 74467-07-5
• Molecular Formula: C₉H₁₀ClNO₃
• Molecular Weight: 215.636
• Mol file: 74467-07-5.mol

Synonyms:2,4-Dimethoxybenzohydroximinoyl chloride

Chemical Property of 2,4-Dimethoxybenzohydroximinoyl chloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,4-Dimethoxybenzohydroximinoyl chloride

There total 3 articles about 2,4-Dimethoxybenzohydroximinoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

2,4-dimethoxybenzaldoxime (31874-34-7) → 2,4-Dimethoxybenzohydroximinoyl chloride (74467-07-5)

Guidance literature:

With hydrogenchloride; Oxone; silica gel; at 20 ℃; for 0.15h;

Reference yield:

2,4-dimethoxybenzaldoxime (31874-34-7) → 5-Chloro-2,4-dimethoxybenzaldehyde oxime (74467-06-4) + 2,4-Dimethoxybenzohydroximinoyl chloride (74467-07-5)

Guidance literature:

With N-chloro-succinimide; In N,N-dimethyl-formamide; Yield given. Yields of byproduct given;

DOI:10.1021/jo01307a039

Reference yield:

→ 2,4-Dimethoxybenzohydroximinoyl chloride (74467-07-5)

Guidance literature:

upstream raw materials:

2,4-dimethoxybenzaldoxime

Refernces

• 1、 Bigdeli, Mohammad A.,Mahdavinia, Gholam Hossein,Jafari, Saeed. "The synthesis of benzhydroximoyl chloride and nitrile oxides under solvent free conditions". . p. 26 - 28. Retrieved 2008/02/02.