2-(2-bromo-3-fluoro-phenoxy)-6-(2-bromo-3-methoxy-phenoxy)-phenylamine

Base Information

Chemical Name:2-(2-bromo-3-fluoro-phenoxy)-6-(2-bromo-3-methoxy-phenoxy)-phenylamine
CAS No.:861885-68-9
Molecular Formula:C₁₉H₁₄Br₂FNO₃
Molecular Weight:483.131
Hs Code.:

Synonyms:2-(2-bromo-3-fluoro-phenoxy)-6-(2-bromo-3-methoxy-phenoxy)-phenylamine

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Chemical Property of 2-(2-bromo-3-fluoro-phenoxy)-6-(2-bromo-3-methoxy-phenoxy)-phenylamine

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Technology Process of 2-(2-bromo-3-fluoro-phenoxy)-6-(2-bromo-3-methoxy-phenoxy)-phenylamine

There total 4 articles about 2-(2-bromo-3-fluoro-phenoxy)-6-(2-bromo-3-methoxy-phenoxy)-phenylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 861885-67-8
C₁₉H₁₂Br₂FNO₅

: 861885-68-9
2-(2-bromo-3-fluoro-phenoxy)-6-(2-bromo-3-methoxy-phenoxy)-phenylamine

Guidance literature:: With 4-bromo-phenol; hydrazine hydrate; palladium on activated charcoal; In ethanol; for 2h; Heating;
DOI:10.1002/anie.200500397

Reference yield:

: 861885-66-7
C₁₃H₉BrFNO₄

: 861885-68-9
2-(2-bromo-3-fluoro-phenoxy)-6-(2-bromo-3-methoxy-phenoxy)-phenylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / NaH / dimethylsulfoxide / 3 h / 130 °C

2: 85 percent / hydrazine hydrate; p-bromophenol / Pd/C / ethanol / 2 h / Heating

With 4-bromo-phenol; sodium hydride; hydrazine hydrate; palladium on activated charcoal; In ethanol; dimethyl sulfoxide;
DOI:10.1002/anie.200500397

Reference yield:

: 19064-24-5
2,6-difluoro-1-nitrobenzene

: 861885-68-9
2-(2-bromo-3-fluoro-phenoxy)-6-(2-bromo-3-methoxy-phenoxy)-phenylamine

Guidance literature:: Multi-step reaction with 3 steps

1: NaH / dimethylsulfoxide / 2.5 h / 130 °C

2: 86 percent / NaH / dimethylsulfoxide / 3 h / 130 °C

3: 85 percent / hydrazine hydrate; p-bromophenol / Pd/C / ethanol / 2 h / Heating

With 4-bromo-phenol; sodium hydride; hydrazine hydrate; palladium on activated charcoal; In ethanol; dimethyl sulfoxide;
DOI:10.1002/anie.200500397