2-<2'-O-benzoyl-3',5'-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranosyl>-N-(benzyloxycarbonyl)-D,L-glycinenitrile

Base Information

Chemical Name:2-<2'-O-benzoyl-3',5'-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranosyl>-N-(benzyloxycarbonyl)-D,L-glycinenitrile
CAS No.:184241-20-1
Molecular Formula:C₃₄H₄₈N₂O₈Si₂
Molecular Weight:668.935
Hs Code.:

Synonyms:2-<2'-O-benzoyl-3',5'-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranosyl>-N-(benzyloxycarbonyl)-D,L-glycinenitrile

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Chemical Property of 2-<2'-O-benzoyl-3',5'-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranosyl>-N-(benzyloxycarbonyl)-D,L-glycinenitrile

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Technology Process of 2-<2'-O-benzoyl-3',5'-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranosyl>-N-(benzyloxycarbonyl)-D,L-glycinenitrile

There total 5 articles about 2-<2'-O-benzoyl-3',5'-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranosyl>-N-(benzyloxycarbonyl)-D,L-glycinenitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: N-(benzyloxycarbonyl)-2-(β-D-ribofuranosyl)-D,L-glycinenitrile

: 184241-20-1
2-<2'-O-benzoyl-3',5'-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranosyl>-N-(benzyloxycarbonyl)-D,L-glycinenitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-imidazole / dimethylformamide / 1.5 h / 0 °C

2: pyridine / 3 h / Ambient temperature

With pyridine; 1H-imidazole; In N,N-dimethyl-formamide;
DOI:10.1002/hlca.19960790710

Reference yield:

: 69304-37-6
1,3-Dichloro-1,1,3,3-tetraisopropyldisiloxane

: 184241-20-1
2-<2'-O-benzoyl-3',5'-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranosyl>-N-(benzyloxycarbonyl)-D,L-glycinenitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-imidazole / dimethylformamide / 1.5 h / 0 °C

2: pyridine / 3 h / Ambient temperature

With pyridine; 1H-imidazole; In N,N-dimethyl-formamide;
DOI:10.1002/hlca.19960790710

Reference yield:

: [Carbamoyl-((2S,3R,4S,5R)-3,4-dihydroxy-5-hydroxymethyl-tetrahydro-furan-2-yl)-methyl]-carbamic acid benzyl ester

: 184241-20-1
2-<2'-O-benzoyl-3',5'-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranosyl>-N-(benzyloxycarbonyl)-D,L-glycinenitrile

Guidance literature:: Multi-step reaction with 3 steps

1: TFAA, pyridine / dioxane

2: imidazole / dimethylformamide

3: pyridine

With pyridine; 1H-imidazole; trifluoroacetic anhydride; In 1,4-dioxane; N,N-dimethyl-formamide;