8-azido-2-cyclohexylquinoline

Base Information

Chemical Name:8-azido-2-cyclohexylquinoline
CAS No.:1336877-52-1
Molecular Formula:C₁₅H₁₆N₄
Molecular Weight:252.319
Hs Code.:

Synonyms:8-azido-2-cyclohexylquinoline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 8-azido-2-cyclohexylquinoline

Chemical Property:

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Technology Process of 8-azido-2-cyclohexylquinoline

There total 3 articles about 8-azido-2-cyclohexylquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1005-07-8
o-azidoaniline

: 1051379-48-6
3-ethoxy-spiro[3.5]nonan-1-one

: 1336877-52-1
8-azido-2-cyclohexylquinoline

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃; for 12h; regioselective reaction; Inert atmosphere;
DOI:10.1021/ol202334s

Reference yield:

: 62-53-3
aniline

: 1336877-52-1
8-azido-2-cyclohexylquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: trimethylsilylazide; copper(I) bromide; tert.-butylhydroperoxide / acetonitrile / 4 h / 30 °C / Inert atmosphere

2: boron trifluoride diethyl etherate / dichloromethane / 20 °C / Inert atmosphere

With tert.-butylhydroperoxide; trimethylsilylazide; boron trifluoride diethyl etherate; copper(I) bromide; In dichloromethane; acetonitrile;
DOI:10.1002/anie.201505898

Reference yield:

: 2719-27-9
cyclohexanylcarbonyl chloride

: 1336877-52-1
8-azido-2-cyclohexylquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / acetonitrile / 3 h / 90 °C

2: boron trifluoride diethyl etherate / dichloromethane / 20 °C / Inert atmosphere

With boron trifluoride diethyl etherate; triethylamine; In dichloromethane; acetonitrile;
DOI:10.1002/anie.201505898