1,10-bis(4-[trans-3-(4-hydroxyphenyl)-3-oxopropenyl]phenyl)-1,4,7,10-tetraoxadecane

Base Information

Chemical Name:1,10-bis(4-[trans-3-(4-hydroxyphenyl)-3-oxopropenyl]phenyl)-1,4,7,10-tetraoxadecane
CAS No.:650625-65-3
Molecular Formula:C₃₆H₃₄O₈
Molecular Weight:594.661
Hs Code.:

Synonyms:1,10-bis(4-[trans-3-(4-hydroxyphenyl)-3-oxopropenyl]phenyl)-1,4,7,10-tetraoxadecane

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Chemical Property of 1,10-bis(4-[trans-3-(4-hydroxyphenyl)-3-oxopropenyl]phenyl)-1,4,7,10-tetraoxadecane

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Technology Process of 1,10-bis(4-[trans-3-(4-hydroxyphenyl)-3-oxopropenyl]phenyl)-1,4,7,10-tetraoxadecane

There total 3 articles about 1,10-bis(4-[trans-3-(4-hydroxyphenyl)-3-oxopropenyl]phenyl)-1,4,7,10-tetraoxadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 111550-48-2
4,4′-(((ethane-1,2-diylbis(oxy))bis(ethane-2,1-diyl))bis(oxy))dibenzaldehyde

: 99-93-4
4-Hydroxyacetophenone

: 650625-65-3
1,10-bis(4-[trans-3-(4-hydroxyphenyl)-3-oxopropenyl]phenyl)-1,4,7,10-tetraoxadecane

Guidance literature:: With sodium hydroxide; In ethanol; water; at 50 ℃; for 48h;
DOI:10.1016/j.tet.2003.10.026

Reference yield:

: 19249-03-7
triethylene glycol di-(p-toluenesulfonate)

: 650625-65-3
1,10-bis(4-[trans-3-(4-hydroxyphenyl)-3-oxopropenyl]phenyl)-1,4,7,10-tetraoxadecane

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / K₂CO₃ / dimethylformamide / 80 °C

2: 86 percent / NaOH / ethanol; H₂O / 48 h / 50 °C

With sodium hydroxide; potassium carbonate; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2003.10.026

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 650625-65-3
1,10-bis(4-[trans-3-(4-hydroxyphenyl)-3-oxopropenyl]phenyl)-1,4,7,10-tetraoxadecane

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / K₂CO₃ / dimethylformamide / 80 °C

2: 86 percent / NaOH / ethanol; H₂O / 48 h / 50 °C

With sodium hydroxide; potassium carbonate; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2003.10.026