Acetic acid (1S,4S)-4-bromo-1-((1S,4S,5S,6R,9S)-9-bromo-6-methyl-11-oxa-tricyclo[4.3.2.0^1,5]undec-4-ylmethyl)-3,3-dimethyl-cyclohexyl ester

Base Information

• Chemical Name: Acetic acid (1S,4S)-4-bromo-1-((1S,4S,5S,6R,9S)-9-bromo-6-methyl-11-oxa-tricyclo[4.3.2.0^1,5]undec-4-ylmethyl)-3,3-dimethyl-cyclohexyl ester
• CAS No.: 83543-88-8
• Molecular Formula: C₂₂H₃₄Br₂O₃
• Molecular Weight: 506.318

Synonyms:Acetic acid (1S,4S)-4-bromo-1-((1S,4S,5S,6R,9S)-9-bromo-6-methyl-11-oxa-tricyclo[4.3.2.0^1,5]undec-4-ylmethyl)-3,3-dimethyl-cyclohexyl ester

Chemical Property of Acetic acid (1S,4S)-4-bromo-1-((1S,4S,5S,6R,9S)-9-bromo-6-methyl-11-oxa-tricyclo[4.3.2.0^1,5]undec-4-ylmethyl)-3,3-dimethyl-cyclohexyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Acetic acid (1S,4S)-4-bromo-1-((1S,4S,5S,6R,9S)-9-bromo-6-methyl-11-oxa-tricyclo[4.3.2.0^1,5]undec-4-ylmethyl)-3,3-dimethyl-cyclohexyl ester

There total 3 articles about Acetic acid (1S,4S)-4-bromo-1-((1S,4S,5S,6R,9S)-9-bromo-6-methyl-11-oxa-tricyclo[4.3.2.0^1,5]undec-4-ylmethyl)-3,3-dimethyl-cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

pinnaterpene A (81474-79-5) → Acetic acid (1S,4S)-4-bromo-1-((1S,4S,5S,6R,9S)-9-bromo-6-methyl-11-oxa-tricyclo[4.3.2.01,5]undec-4-ylmethyl)-3,3-dimethyl-cyclohexyl ester (83543-88-8)

Guidance literature:

With lead(IV) acetate; iodine; In benzene; for 48h; Heating;

DOI:10.1246/cl.1982.1389

Reference yield: 26.0%

pinnaterpene B (81474-78-4) → Acetic acid (1S,4S)-4-bromo-1-((1S,4S,5S,6R,9S)-9-bromo-6-methyl-11-oxa-tricyclo[4.3.2.01,5]undec-4-ylmethyl)-3,3-dimethyl-cyclohexyl ester (83543-88-8)

Guidance literature:

With p-toluenesulfonyl chloride; In pyridine; 20 deg C, 2 d; 40 deg C, 1 d; 60 deg C, 1 d; reflux, 1 d;

DOI:10.1246/cl.1982.1389

Reference yield:

pinnaterpene C (81474-77-3) → Acetic acid (1S,4S)-4-bromo-1-((1S,4S,5S,6R,9S)-9-bromo-6-methyl-11-oxa-tricyclo[4.3.2.01,5]undec-4-ylmethyl)-3,3-dimethyl-cyclohexyl ester (83543-88-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 65 percent / sodium borohydride / ethanol / 48 h / Ambient temperature

2: 26 percent / tosyl chloride / pyridine / 20 deg C, 2 d; 40 deg C, 1 d; 60 deg C, 1 d; reflux, 1 d

With sodium tetrahydroborate; p-toluenesulfonyl chloride; In pyridine; ethanol;

DOI:10.1246/cl.1982.1389

upstream raw materials:

pinnaterpene A

pinnaterpene B

pinnaterpene C

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 83543-88-8 Acetic acid (1S,4S)-4-bromo-1-((1S,4S,5S,6R,9S)-9-bromo-6-methyl-11-oxa-tricyclo[4.3.2.0^1,5]undec-4-ylmethyl)-3,3-dimethyl-cyclohexyl ester

Send

Send

Metric Ton KG G Pound L ML

Send

Send