ethyl 2-(2-{[4-(1-benzofuran-2-yl)benzoyl]amino}ethyl)-5-phenylpentanoate

Base Information

Chemical Name:ethyl 2-(2-{[4-(1-benzofuran-2-yl)benzoyl]amino}ethyl)-5-phenylpentanoate
CAS No.:905291-54-5
Molecular Formula:C₃₀H₃₁NO₄
Molecular Weight:469.58
Hs Code.:

Synonyms:ethyl 2-(2-{[4-(1-benzofuran-2-yl)benzoyl]amino}ethyl)-5-phenylpentanoate

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Chemical Property of ethyl 2-(2-{[4-(1-benzofuran-2-yl)benzoyl]amino}ethyl)-5-phenylpentanoate

Chemical Property:

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Technology Process of ethyl 2-(2-{[4-(1-benzofuran-2-yl)benzoyl]amino}ethyl)-5-phenylpentanoate

There total 6 articles about ethyl 2-(2-{[4-(1-benzofuran-2-yl)benzoyl]amino}ethyl)-5-phenylpentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 905291-53-4
ethyl (4E)-2-(2-{[4-(1-benzofuran-2-yl)benzoyl]amino}ethyl)-5-phenyl-4-pentenoate

: 905291-54-5
ethyl 2-(2-{[4-(1-benzofuran-2-yl)benzoyl]amino}ethyl)-5-phenylpentanoate

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; at 20 ℃; for 0.5h; atmospheric pressure;
DOI:10.1016/j.bmc.2006.03.032

Reference yield:

: 380470-00-8
ethyl 4-[(4-iodobenzoyl)amino]butanoate

: 905291-54-5
ethyl 2-(2-{[4-(1-benzofuran-2-yl)benzoyl]amino}ethyl)-5-phenylpentanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium hexamethyldisilazide / tetrahydrofuran / 1 h / cooling

1.2: 67 percent / tetrahydrofuran / 2 h / cooling

2.1: 95 percent / triethylamine / dichloro(triphenylphosphine)palladium(II) / dimethylformamide / 6 h / 80 °C

3.1: hydrogen / palladium on carbon / methanol / 0.5 h / 20 °C / atmospheric pressure

With hydrogen; triethylamine; lithium hexamethyldisilazane; palladium on activated charcoal; dichloro(triphenylphosphine)palladium(II); In tetrahydrofuran; methanol; N,N-dimethyl-formamide; 2.1: Suzuki coupling;
DOI:10.1016/j.bmc.2006.03.032

Reference yield:

: 905291-52-3
ethyl (4E)-2-{2-[(4-iodobenzoyl)amino]ethyl}-5-phenyl-4-pentenoate

: 905291-54-5
ethyl 2-(2-{[4-(1-benzofuran-2-yl)benzoyl]amino}ethyl)-5-phenylpentanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / triethylamine / dichloro(triphenylphosphine)palladium(II) / dimethylformamide / 6 h / 80 °C

2: hydrogen / palladium on carbon / methanol / 0.5 h / 20 °C / atmospheric pressure

With hydrogen; triethylamine; palladium on activated charcoal; dichloro(triphenylphosphine)palladium(II); In methanol; N,N-dimethyl-formamide; 1: Suzuki coupling;
DOI:10.1016/j.bmc.2006.03.032