2-methylvaleryl chloride

Base Information

Chemical Name:2-methylvaleryl chloride
CAS No.:116908-84-0
Molecular Formula:C₆H₁₁ClO
Molecular Weight:134.606
Hs Code.:

Synonyms:2-methylvaleryl chloride

Suppliers and Price of 2-methylvaleryl chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-methylvaleryl chloride

Chemical Property:

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Technology Process of 2-methylvaleryl chloride

There total 4 articles about 2-methylvaleryl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 97-61-0,22160-39-0
2-Methylpentanoic acid

: 116908-84-0,5238-27-7
2-methylvaleryl chloride

Guidance literature:: With thionyl chloride;
DOI:10.1021/ja00812a040 DOI:10.1021/jo01033a054

Reference yield:

: 7719-09-7
thionyl chloride

: 97-61-0,22160-39-0
2-Methylpentanoic acid

: 116908-84-0,5238-27-7
2-methylvaleryl chloride

Guidance literature:: In dichloromethane; at 25 ℃; for 12h;
DOI:10.1021/jm901229s

Reference yield:

: 109-52-4
valeric acid

: 116908-84-0,5238-27-7
2-methylvaleryl chloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium; diisopropylamine / tetrahydrofuran; hexane / 1 h / -15 °C

1.2: -15 - 20 °C

2.1: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 0 - 20 °C

With n-butyllithium; oxalyl dichloride; diisopropylamine; N,N-dimethyl-formamide; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1002/anie.202013275