2-(hydroxy-phenyl-methyl)-naphthalene-1-carboxylic acid bis-(1-propyl-butyl)-amide

Base Information

• Chemical Name: 2-(hydroxy-phenyl-methyl)-naphthalene-1-carboxylic acid bis-(1-propyl-butyl)-amide
• CAS No.: 286366-50-5
• Molecular Formula: C₃₂H₄₃NO₂
• Molecular Weight: 473.699

Synonyms:2-(hydroxy-phenyl-methyl)-naphthalene-1-carboxylic acid bis-(1-propyl-butyl)-amide

Chemical Property of 2-(hydroxy-phenyl-methyl)-naphthalene-1-carboxylic acid bis-(1-propyl-butyl)-amide

Chemical Property:

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Technology Process of 2-(hydroxy-phenyl-methyl)-naphthalene-1-carboxylic acid bis-(1-propyl-butyl)-amide

There total 2 articles about 2-(hydroxy-phenyl-methyl)-naphthalene-1-carboxylic acid bis-(1-propyl-butyl)-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

phenylmagnesium bromide + 2-Formyl-N,N-bis(1-propylbutyl)-1-naphthamide (197587-50-1) → 2-(hydroxy-phenyl-methyl)-naphthalene-1-carboxylic acid bis-(1-propyl-butyl)-amide (286366-50-5)

Guidance literature:

In tetrahydrofuran; at -78 ℃; for 3h;

DOI:10.1039/b000669f

Reference yield:

2-Benzoyl-N,N-bis(4-heptyl)-1-naphthamide → 2-(hydroxy-phenyl-methyl)-naphthalene-1-carboxylic acid bis-(1-propyl-butyl)-amide (286366-50-5)

Guidance literature:

With lithium triethylborohydride; In tetrahydrofuran; at 0 ℃; for 2h;

DOI:10.1039/b000668h

Reference yield: 86.0%

2-(hydroxy-phenyl-methyl)-naphthalene-1-carboxylic acid bis-(1-propyl-butyl)-amide (286366-50-5) → 2-Benzoyl-N,N-bis(4-heptyl)-1-naphthamide

Guidance literature:

With chromium(VI) oxide; sulfuric acid; In water; acetone; at 0 - 20 ℃; for 1.16667h;

DOI:10.1039/b000668h

upstream raw materials:

2-Formyl-N,N-bis(1-propylbutyl)-1-naphthamide

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