Cyclobutane, 1,3-dimethyl-, cis-

Base Information

• Chemical Name: Cyclobutane, 1,3-dimethyl-, cis-
• CAS No.: 2398-09-6
• Molecular Formula: C₆H₁₂
• Molecular Weight: 84.1613
• Mol file: 2398-09-6.mol

Synonyms:cis-1,3-Dimethylcyclobutane

Chemical Property of Cyclobutane, 1,3-dimethyl-, cis-

Chemical Property:

• Vapor Pressure: 166mmHg at 25°C
• Melting Point: -132.62°C (estimate)
• Refractive Index: 1.416
• Boiling Point: 66.1°C at 760 mmHg
• PSA: 0.00000
• Density: 0.758g/cm³
• LogP: 2.05240

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Cyclobutane, 1,3-dimethyl-, cis-

There total 3 articles about Cyclobutane, 1,3-dimethyl-, cis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cis-1,3-bis(hydroxymethyl)cyclobutane ditosylate (2602-14-4) → cis-1,3-Dimethyl-cyclobutan (2398-09-6)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether;

DOI:10.1021/jo01017a057 DOI:10.1002/mrc.1270130308

Reference yield:

3-methyl-cyclobutanecarbaldehyde (872286-84-5) → trans-1,3-dimethylcyclobutane (2398-10-9) + cis-1,3-Dimethyl-cyclobutan (2398-09-6)

Guidance literature:

With potassium hydroxide; platinum on activated charcoal;

Reference yield:

→ cis-1,3-Dimethyl-cyclobutan (2398-09-6)

Guidance literature:

trans-1,3-Dibrom-1,3-dimethyl-cyclobutan, Tributyl-zinn-hydrid; Gem. m. trans-Isomer;

DOI:10.1021/ja01065a051

upstream raw materials:

3-methyl-cyclobutanecarbaldehyde

cis-1,3-bis(hydroxymethyl)cyclobutane ditosylate