2,3-Dihydro-1-benzofuran-2-carbonyl chloride

Base Information

Chemical Name:2,3-Dihydro-1-benzofuran-2-carbonyl chloride
CAS No.:27347-32-6
Molecular Formula:C9H7 Cl O2
Molecular Weight:182.606
Hs Code.:2932999099
European Community (EC) Number:692-343-3
DSSTox Substance ID:DTXSID20383665
Mol file:27347-32-6.mol

Synonyms:27347-32-6;2,3-dihydro-1-benzofuran-2-carbonyl chloride;2,3-dihydrobenzofuran-2-carbonyl chloride;2,3-Dihydro-benzofuran-2-carbonyl chloride;2-Benzofurancarbonylchloride, 2,3-dihydro-;2,3-dihydrobenzo[b]furan-2-carbonyl chloride;2,3-Dihydro-1-benzofuran-2-carbonyl chloride, 95%;SCHEMBL2176045;DTXSID20383665;QZVPHVMVWZKULP-UHFFFAOYSA-N;CBA34732;STR07068;MFCD03086169;AKOS009216234;FT-0609643;2,3-DIHYDRO-1-BENZOFURAN-2-CARBONYLCHLORIDE;J-507009

Suppliers and Price of 2,3-Dihydro-1-benzofuran-2-carbonyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2,3-Dihydro-benzofuran-2-carbonylChloride
100mg
$ 175.00

SynQuest Laboratories
2,3-Dihydrobenzofuran-2-carbonylchloride
500 mg
$ 221.00

SynQuest Laboratories
2,3-Dihydrobenzofuran-2-carbonylchloride
1 g
$ 349.00

Matrix Scientific
2,3-Dihydro-benzofuran-2-carbonylchloride 95%+
500mg
$ 342.00

Matrix Scientific
2,3-Dihydro-benzofuran-2-carbonylchloride 95%+
1g
$ 540.00

American Custom Chemicals Corporation
2,3-DIHYDRO-1-BENZOFURAN-2-CARBONYL CHLORIDE 95.00%
1G
$ 1112.10

American Custom Chemicals Corporation
2,3-DIHYDRO-1-BENZOFURAN-2-CARBONYL CHLORIDE 95.00%
250MG
$ 722.80

Advanced Chemicals Intermediatesced Chemicals Intermediates
2,3-Dihydro-benzofuran-2-carbonylchloride 95%+
500mg
$ 137.75

Acints
2,3-Dihydro-benzofuran-2-carbonylchloride 95%+
5g
$ 717.75

Acints
2,3-Dihydro-benzofuran-2-carbonylchloride 95%+
1g
$ 217.50

Total 5 raw suppliers

Chemical Property of 2,3-Dihydro-1-benzofuran-2-carbonyl chloride

Chemical Property:

Vapor Pressure:0.00683mmHg at 25°C
Refractive Index:1.575
Boiling Point:270.5°Cat760mmHg
Flash Point:100.8°C
PSA：26.30000
Density:1.345g/cm³
LogP:1.75550
XLogP3:2.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:182.0134572
Heavy Atom Count:12
Complexity:193

Purity/Quality:

98%min ^*data from raw suppliers

2,3-Dihydro-benzofuran-2-carbonylChloride ^*data from reagent suppliers

Safty Information:

Pictogram(s): R34:Causes burns.;
Hazard Codes: C:Corrosive;
Statements: 34
Safety Statements: 26-36/37/39

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1C(OC2=CC=CC=C21)C(=O)Cl

Technology Process of 2,3-Dihydro-1-benzofuran-2-carbonyl chloride

There total 7 articles about 2,3-Dihydro-1-benzofuran-2-carbonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1914-60-9
2,3-dihydro-1-benzofuran-2-carboxylic acid

: 27347-32-6
2,3-dihydrobenzofuran-2-carbonyl chloride

Guidance literature:: With thionyl chloride; In benzene; for 2.5h; Heating;
DOI:10.1021/jm00371a003

Reference yield:

: 66158-96-1
2-hydroxymethyl-1H-2,3-dihydrobenzofuran

: 27347-32-6
2,3-dihydrobenzofuran-2-carbonyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; potassium bromide; sodium hypochlorite / tetrahydrofuran; water / 3 h / 20 °C

2: thionyl chloride / 6 h / 60 °C

With sodium hypochlorite; thionyl chloride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hydrogencarbonate; potassium bromide; In tetrahydrofuran; water;
DOI:10.1055/s-0036-1588998

Reference yield:

: 1745-81-9
o-Allylphenol

: 27347-32-6
2,3-dihydrobenzofuran-2-carbonyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: dihydrogen peroxide; 2,2,2-Trifluoroacetophenone / tert-butyl alcohol; acetonitrile / 18 h / 20 °C / Green chemistry

1.2: 1 h / 60 °C / Green chemistry

2.1: sodium hydrogencarbonate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; potassium bromide; sodium hypochlorite / tetrahydrofuran; water / 3 h / 20 °C

3.1: thionyl chloride / 6 h / 60 °C

With sodium hypochlorite; thionyl chloride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; 2,2,2-Trifluoroacetophenone; dihydrogen peroxide; sodium hydrogencarbonate; potassium bromide; In tetrahydrofuran; water; acetonitrile; tert-butyl alcohol;
DOI:10.1055/s-0036-1588998