(E)-4-[(N-tert-butoxycarbonylaminoethyl)-N-benzyloxycarbonylamino]-2-butenal

Base Information

Chemical Name:(E)-4-[(N-tert-butoxycarbonylaminoethyl)-N-benzyloxycarbonylamino]-2-butenal
CAS No.:1000806-56-3
Molecular Formula:C₁₉H₂₆N₂O₅
Molecular Weight:362.426
Hs Code.:

Synonyms:(E)-4-[(N-tert-butoxycarbonylaminoethyl)-N-benzyloxycarbonylamino]-2-butenal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-4-[(N-tert-butoxycarbonylaminoethyl)-N-benzyloxycarbonylamino]-2-butenal

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Technology Process of (E)-4-[(N-tert-butoxycarbonylaminoethyl)-N-benzyloxycarbonylamino]-2-butenal

There total 1 articles about (E)-4-[(N-tert-butoxycarbonylaminoethyl)-N-benzyloxycarbonylamino]-2-butenal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 1000806-47-2
N-allyl-N-benzyloxycarbonyl-N'-tert-butoxycarbonyl-ethylenediamine

: 107-02-8,25068-14-8
acrolein

: 1000806-56-3
(E)-4-[(N-tert-butoxycarbonylaminoethyl)-N-benzyloxycarbonylamino]-2-butenal

Guidance literature:: [1,3-bis-(2,4,6-trimethylphenyl)-2-imidazolidinylidene]dichloro(O-isopropoxyphenylmethylene)ruthenium; In dichloromethane; at 20 ℃; for 15h;
DOI:10.1021/ol702447y

Reference yield:

: 1000806-56-3
(E)-4-[(N-tert-butoxycarbonylaminoethyl)-N-benzyloxycarbonylamino]-2-butenal

: 947275-75-4
(5R)-(1-benzyloxycarbonyl)-4-tert-butoxycarbonyl-5-(2-hydroxyethyl)piperazine

: 183591-29-9
(5S)-(1-benzyloxycarbonyl)-4-tert-butoxycarbonyl-5-(2-hydroxyethyl)piperazine

Guidance literature:: (E)-4-[(N-tert-butoxycarbonylaminoethyl)-N-benzyloxycarbonylamino]-2-butenal; With benzoic acid; In chloroform; at -50 - -40 ℃; for 62h;

With sodium tetrahydroborate; In methanol; chloroform; at 0 ℃; for 0.5h; Further stages. Title compound not separated from byproducts.;
DOI:10.1021/ol702447y