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β-benzyl N-phosphonoacetyl-L-isoasparaginate

Base Information Edit
  • Chemical Name:β-benzyl N-phosphonoacetyl-L-isoasparaginate
  • CAS No.:913094-95-8
  • Molecular Formula:C13H17N2O7P
  • Molecular Weight:344.261
  • Hs Code.:
  • Mol file:913094-95-8.mol
β-benzyl N-phosphonoacetyl-L-isoasparaginate

Synonyms:β-benzyl N-phosphonoacetyl-L-isoasparaginate

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Chemical Property of β-benzyl N-phosphonoacetyl-L-isoasparaginate Edit
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Technology Process of β-benzyl N-phosphonoacetyl-L-isoasparaginate

There total 6 articles about β-benzyl N-phosphonoacetyl-L-isoasparaginate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
β-benzyl N-(diethoxyphosphinoyl)acetyl-L-isoasparaginate; With trimethylsilyl bromide; In acetonitrile; at 20 ℃;
With water; at 20 ℃; for 1h;
DOI:10.1021/jm0607294
Guidance literature:
Multi-step reaction with 2 steps
1.1: 95 percent / 8 h / 150 °C
2.1: trimethylsilyl bromide / acetonitrile / 20 °C
2.2: 100 percent / H2O / 1 h / 20 °C
With trimethylsilyl bromide; In acetonitrile;
DOI:10.1021/jm0607294
Guidance literature:
Multi-step reaction with 4 steps
1.1: trifluoroacetic acid / CH2Cl2 / 4 h / 20 °C
2.1: 80 percent / pyridine / CH2Cl2 / 4 h / 20 °C
3.1: 95 percent / 8 h / 150 °C
4.1: trimethylsilyl bromide / acetonitrile / 20 °C
4.2: 100 percent / H2O / 1 h / 20 °C
With pyridine; trimethylsilyl bromide; trifluoroacetic acid; In dichloromethane; acetonitrile;
DOI:10.1021/jm0607294
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