di-tert-butyl 2,2'-((5-((trimethylsilyl)ethynyl)-1,3-phenylene)bis(oxy))diacetate

Base Information

Chemical Name:di-tert-butyl 2,2'-((5-((trimethylsilyl)ethynyl)-1,3-phenylene)bis(oxy))diacetate
CAS No.:1425510-02-6
Molecular Formula:C₂₃H₃₄O₆Si
Molecular Weight:434.605
Hs Code.:

Synonyms:di-tert-butyl 2,2'-((5-((trimethylsilyl)ethynyl)-1,3-phenylene)bis(oxy))diacetate

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Chemical Property of di-tert-butyl 2,2'-((5-((trimethylsilyl)ethynyl)-1,3-phenylene)bis(oxy))diacetate

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Technology Process of di-tert-butyl 2,2'-((5-((trimethylsilyl)ethynyl)-1,3-phenylene)bis(oxy))diacetate

There total 4 articles about di-tert-butyl 2,2'-((5-((trimethylsilyl)ethynyl)-1,3-phenylene)bis(oxy))diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1425510-01-5
di-tert-butyl 2,2'-((5-bromo-1,3-phenylene)bis(oxy))diacetate

: 1066-54-2
trimethylsilylacetylene

: 1425510-02-6
di-tert-butyl 2,2'-((5-((trimethylsilyl)ethynyl)-1,3-phenylene)bis(oxy))diacetate

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diethylamine; triphenylphosphine; In N,N-dimethyl-formamide; at 120 ℃; for 0.5h; Inert atmosphere; Microwave irradiation; Sealed tube;

Reference yield:

: 106120-04-1
5-bromoresorcinol

: 1425510-02-6
di-tert-butyl 2,2'-((5-((trimethylsilyl)ethynyl)-1,3-phenylene)bis(oxy))diacetate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 50 °C / Inert atmosphere

2: diethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triphenylphosphine / N,N-dimethyl-formamide / 0.5 h / 120 °C / Inert atmosphere; Microwave irradiation; Sealed tube

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; potassium carbonate; diethylamine; triphenylphosphine; In N,N-dimethyl-formamide;

Reference yield:

: 5292-43-3
bromoacetic acid tert-butyl ester

: 1425510-02-6
di-tert-butyl 2,2'-((5-((trimethylsilyl)ethynyl)-1,3-phenylene)bis(oxy))diacetate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 50 °C / Inert atmosphere

2: diethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triphenylphosphine / N,N-dimethyl-formamide / 0.5 h / 120 °C / Inert atmosphere; Microwave irradiation; Sealed tube

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; potassium carbonate; diethylamine; triphenylphosphine; In N,N-dimethyl-formamide;