8-methoxy-4-phenoxy-1,2-di(thiophen-3-yl)-3H-pyrrolo-[3,2,1-de]acridin-3-one

Base Information

Chemical Name:8-methoxy-4-phenoxy-1,2-di(thiophen-3-yl)-3H-pyrrolo-[3,2,1-de]acridin-3-one
CAS No.:1434152-90-5
Molecular Formula:C₃₀H₁₉NO₃S₂
Molecular Weight:505.618
Hs Code.:

Synonyms:8-methoxy-4-phenoxy-1,2-di(thiophen-3-yl)-3H-pyrrolo-[3,2,1-de]acridin-3-one

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Chemical Property of 8-methoxy-4-phenoxy-1,2-di(thiophen-3-yl)-3H-pyrrolo-[3,2,1-de]acridin-3-one

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Technology Process of 8-methoxy-4-phenoxy-1,2-di(thiophen-3-yl)-3H-pyrrolo-[3,2,1-de]acridin-3-one

There total 2 articles about 8-methoxy-4-phenoxy-1,2-di(thiophen-3-yl)-3H-pyrrolo-[3,2,1-de]acridin-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1434153-21-5
4-iodo-1,8-dimethoxy-3-(phenoxymethyl)-1H-pyrano[4,3-b]quinoline

: 197957-65-6
1,2-di(thiophen-3-yl)ethyne

: 1434152-90-5
8-methoxy-4-phenoxy-1,2-di(thiophen-3-yl)-3H-pyrrolo-[3,2,1-de]acridin-3-one

Guidance literature:: With sodium acetate; palladium diacetate; lithium chloride; In N,N-dimethyl-formamide; at 120 ℃; for 0.333333h; regioselective reaction; Microwave irradiation;
DOI:10.1021/jo400539x

Reference yield:

: 1434153-28-2
6-methoxy-2-(3-phenoxyprop-1-yn-1-yl)quinoline-3-carbaldehyde

: 1434152-90-5
8-methoxy-4-phenoxy-1,2-di(thiophen-3-yl)-3H-pyrrolo-[3,2,1-de]acridin-3-one

Guidance literature:: Multi-step reaction with 2 steps

1: iodine; potassium carbonate / dichloromethane / 20 °C

2: palladium diacetate; sodium acetate; lithium chloride / N,N-dimethyl-formamide / 0.33 h / 120 °C / Microwave irradiation

With iodine; sodium acetate; palladium diacetate; potassium carbonate; lithium chloride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo400539x