C₂₉H₄₉NO₅SSi

Base Information

Chemical Name:C₂₉H₄₉NO₅SSi
CAS No.:1380242-18-1
Molecular Formula:C₂₉H₄₉NO₅SSi
Molecular Weight:551.863
Hs Code.:

C<sub>29</sub>H<sub>49</sub>NO<sub>5</sub>SSi

Synonyms:C₂₉H₄₉NO₅SSi

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₉H₄₉NO₅SSi

Chemical Property:

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Technology Process of C₂₉H₄₉NO₅SSi

There total 5 articles about C₂₉H₄₉NO₅SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1380242-17-0
C₈H₁₃NO₂S

: 1380242-27-2
C₂₁H₃₆O₃Si

: 1380242-18-1
C₂₉H₄₉NO₅SSi

Guidance literature:: With titanium tetrachloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; at -78 ℃; for 4h; Inert atmosphere;
DOI:10.1002/anie.201201395

Reference yield:

: 69739-34-0
t-butyldimethylsiyl triflate

: 1380242-18-1
C₂₉H₄₉NO₅SSi

Guidance literature:: Multi-step reaction with 3 steps

1: 2,6-dimethylpyridine / dichloromethane / 1 h / 0 °C

2: diisobutylaluminium hydride / dichloromethane; cyclohexane / 3 h / -78 °C / Inert atmosphere

3: titanium tetrachloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 4 h / -78 °C / Inert atmosphere

With 2,6-dimethylpyridine; titanium tetrachloride; diisobutylaluminium hydride; N-ethyl-N,N-diisopropylamine; In dichloromethane; cyclohexane;
DOI:10.1002/anie.201201395

Reference yield:

: 1380242-15-8
C₂₅H₃₁NO₄S

: 1380242-18-1
C₂₉H₄₉NO₅SSi

Guidance literature:: Multi-step reaction with 3 steps

1: 2,6-dimethylpyridine / dichloromethane / 1 h / 0 °C

2: diisobutylaluminium hydride / dichloromethane; cyclohexane / 3 h / -78 °C / Inert atmosphere

3: titanium tetrachloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 4 h / -78 °C / Inert atmosphere

With 2,6-dimethylpyridine; titanium tetrachloride; diisobutylaluminium hydride; N-ethyl-N,N-diisopropylamine; In dichloromethane; cyclohexane;
DOI:10.1002/anie.201201395