C₃₂H₄₈O₆Si

Base Information

Chemical Name:C₃₂H₄₈O₆Si
CAS No.:219780-81-1
Molecular Formula:C₃₂H₄₈O₆Si
Molecular Weight:556.815
Hs Code.:

C<sub>32</sub>H<sub>48</sub>O<sub>6</sub>Si

Synonyms:C₃₂H₄₈O₆Si

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Chemical Property of C₃₂H₄₈O₆Si

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Technology Process of C₃₂H₄₈O₆Si

There total 25 articles about C₃₂H₄₈O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 219780-49-1
C₃₂H₄₆O₆Si

: 219780-81-1
C₃₂H₄₈O₆Si

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; samarium diiodide; In tetrahydrofuran; methanol;
DOI:10.1021/ja9824932

Reference yield:

: 219780-47-9
C₃₉H₆₂O₆Si₂

: 219780-81-1
C₃₂H₄₈O₆Si

Guidance literature:: Multi-step reaction with 8 steps

1: 66 percent / diethyl zinc / toluene; hexane / 0.5 h / 0 °C

2: 77 percent / Dess-Martin periodinane / CH₂Cl₂ / 12 h / 20 °C

3: 84 percent / H₂ / Pd(OH)2 / ethanol / 0.5 h / 20 °C

4: pyridine / CH₂Cl₂ / 2 h / -45 °C

5: 0.742 g / TBAF; AcOH / tetrahydrofuran / 2.5 h / 20 °C

6: 86 percent / pyridinium p-toluenesulfonate / benzene / 1 h / Heating

7: 100 percent / K₂CO₃ / tetrahydrofuran; methanol / 1 h / 20 °C

8: 100 percent / SmI₂; methanol / tetrahydrofuran; hexamethylphosphoric acid triamide / 5 h / 20 °C

With pyridine; methanol; samarium diiodide; tetrabutyl ammonium fluoride; hydrogen; diethylzinc; pyridinium p-toluenesulfonate; potassium carbonate; Dess-Martin periodane; acetic acid; palladium dihydroxide; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; ethanol; hexane; dichloromethane; toluene; benzene; 1: Cycloaddition / 2: Dess-Martin oxidation / 3: Hydrogenolysis / 4: cyclocondensation / 5: desilylation / 6: cyclocondensation / 7: Ring cleavage / 8: Ring cleavage;
DOI:10.1021/ja9939439

Reference yield:

: 219780-48-0
C₄₀H₆₂O₆Si₂

: 219780-81-1
C₃₂H₄₈O₆Si

Guidance literature:: Multi-step reaction with 6 steps

1: 84 percent / H₂ / Pd(OH)2 / ethanol / 0.5 h / 20 °C

2: pyridine / CH₂Cl₂ / 2 h / -45 °C

3: 0.742 g / TBAF; AcOH / tetrahydrofuran / 2.5 h / 20 °C

4: 86 percent / pyridinium p-toluenesulfonate / benzene / 1 h / Heating

5: 100 percent / K₂CO₃ / tetrahydrofuran; methanol / 1 h / 20 °C

6: 100 percent / SmI₂; methanol / tetrahydrofuran; hexamethylphosphoric acid triamide / 5 h / 20 °C

With pyridine; methanol; samarium diiodide; tetrabutyl ammonium fluoride; hydrogen; pyridinium p-toluenesulfonate; potassium carbonate; acetic acid; palladium dihydroxide; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; ethanol; dichloromethane; benzene; 1: Hydrogenolysis / 2: cyclocondensation / 3: desilylation / 4: cyclocondensation / 5: Ring cleavage / 6: Ring cleavage;
DOI:10.1021/ja9939439