4-methoxyphenyl O-(methyl 2,3,4-tri-O-benzoyl-β-D-glucopyranosyluronate)-(1->3)-(2-O-benzoyl-β-D-galactopyranosyl)-(1->3)-2-O-benzoyl-β-D-galactopyranoside

Base Information

• Chemical Name: 4-methoxyphenyl O-(methyl 2,3,4-tri-O-benzoyl-β-D-glucopyranosyluronate)-(1->3)-(2-O-benzoyl-β-D-galactopyranosyl)-(1->3)-2-O-benzoyl-β-D-galactopyranoside
• CAS No.: 677767-26-9
• Molecular Formula: C₆₁H₅₈O₂₃
• Molecular Weight: 1159.12

Synonyms:4-methoxyphenyl O-(methyl 2,3,4-tri-O-benzoyl-β-D-glucopyranosyluronate)-(1->3)-(2-O-benzoyl-β-D-galactopyranosyl)-(1->3)-2-O-benzoyl-β-D-galactopyranoside

Chemical Property of 4-methoxyphenyl O-(methyl 2,3,4-tri-O-benzoyl-β-D-glucopyranosyluronate)-(1->3)-(2-O-benzoyl-β-D-galactopyranosyl)-(1->3)-2-O-benzoyl-β-D-galactopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Useful:

Technology Process of 4-methoxyphenyl O-(methyl 2,3,4-tri-O-benzoyl-β-D-glucopyranosyluronate)-(1->3)-(2-O-benzoyl-β-D-galactopyranosyl)-(1->3)-2-O-benzoyl-β-D-galactopyranoside

There total 1 articles about 4-methoxyphenyl O-(methyl 2,3,4-tri-O-benzoyl-β-D-glucopyranosyluronate)-(1->3)-(2-O-benzoyl-β-D-galactopyranosyl)-(1->3)-2-O-benzoyl-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

4-methoxyphenyl O-(methyl 2,3,4-tri-O-benzoyl-β-D-glucopyranosyluronate)-(1->3)-(2-O-benzoyl-β-D-galactopyranosyl)-(1->3)-2-O-benzoyl-4,6-O-benzylidene-β-D-galactopyranoside (677767-23-6) → 4-methoxyphenyl O-(methyl 2,3,4-tri-O-benzoyl-β-D-glucopyranosyluronate)-(1->3)-(2-O-benzoyl-β-D-galactopyranosyl)-(1->3)-2-O-benzoyl-β-D-galactopyranoside (677767-26-9)

Guidance literature:

With trifluoroacetic acid; at 20 ℃; for 0.25h;

DOI:10.1039/b314244b

Reference yield:

4-methoxyphenyl O-(methyl 2,3,4-tri-O-benzoyl-β-D-glucopyranosyluronate)-(1->3)-(2-O-benzoyl-β-D-galactopyranosyl)-(1->3)-2-O-benzoyl-β-D-galactopyranoside (677767-26-9) → 6-{2-[3,5-dihydroxy-2-hydroxymethyl-6-(4-methoxy-phenoxy)-tetrahydro-pyran-4-yloxy]-3,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-4-yloxy}-3,4,5-trihydroxy-tetrahydro-pyran-2-carboxylic acid methyl ester

Guidance literature:

With lithium hydroxide; dihydrogen peroxide; In tetrahydrofuran; at 0 - 20 ℃; for 6h;

DOI:10.1039/b314244b

Reference yield:

4-methoxyphenyl O-(methyl 2,3,4-tri-O-benzoyl-β-D-glucopyranosyluronate)-(1->3)-(2-O-benzoyl-β-D-galactopyranosyl)-(1->3)-2-O-benzoyl-β-D-galactopyranoside (677767-26-9) → 3,4,5-tris-benzoyloxy-6-{3-benzoyloxy-2-[3-benzoyloxy-5-hydroxy-2-(4-methoxy-phenoxy)-6-sulfooxymethyl-tetrahydro-pyran-4-yloxy]-5-hydroxy-6-sulfooxymethyl-tetrahydro-pyran-4-yloxy}-tetrahydro-pyran-2-carboxylic acid methyl ester (744196-54-1)

Guidance literature:

With sulfur trioxide trimethylamine complex; In N,N-dimethyl-formamide; at 40 ℃; for 1.5h;

DOI:10.1039/b314244b

upstream raw materials:

4-methoxyphenyl O-(methyl 2,3,4-tri-O-benzoyl-β-D-glucopyranosyluronate)-(1->3)-(2-O-benzoyl-β-D-galactopyranosyl)-(1->3)-2-O-benzoyl-4,6-O-benzylidene-β-D-galactopyranoside

Downstream raw materials:

3,4,5-tris-benzoyloxy-6-{3-benzoyloxy-2-[3-benzoyloxy-5-hydroxy-6-hydroxymethyl-2-(4-methoxy-phenoxy)-tetrahydro-pyran-4-yloxy]-5-hydroxy-6-sulfooxymethyl-tetrahydro-pyran-4-yloxy}-tetrahydro-pyran-2-carboxylic acid methyl ester

3,4,5-tris-benzoyloxy-6-{3-benzoyloxy-2-[3-benzoyloxy-5-hydroxy-2-(4-methoxy-phenoxy)-6-sulfooxymethyl-tetrahydro-pyran-4-yloxy]-5-hydroxy-6-hydroxymethyl-tetrahydro-pyran-4-yloxy}-tetrahydro-pyran-2-carboxylic acid methyl ester

3,4,5-tris-benzoyloxy-6-{3-benzoyloxy-2-[3-benzoyloxy-5-hydroxy-2-(4-methoxy-phenoxy)-6-sulfooxymethyl-tetrahydro-pyran-4-yloxy]-5-hydroxy-6-sulfooxymethyl-tetrahydro-pyran-4-yloxy}-tetrahydro-pyran-2-carboxylic acid methyl ester

(2S,3S,4S,5R,6R)-6-{(2S,3R,4S,5S,6R)-2-[(2R,3S,4S,5R,6S)-3,5-Dihydroxy-2-hydroxymethyl-6-(4-methoxy-phenoxy)-tetrahydro-pyran-4-yloxy]-3,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-4-yloxy}-3,4,5-trihydroxy-tetrahydro-pyran-2-carboxylic acid

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