Technology Process of C47H47FO8
There total 5 articles about C47H47FO8 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
at 20 ℃;
for 14h;
Inert atmosphere;
DOI:10.1039/c2cc33704e
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 1H-imidazole / N,N-dimethyl-formamide / 2 h / 0 °C / Inert atmosphere
2.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / -78 °C / Inert atmosphere
2.2: 0.25 h / -78 °C / Inert atmosphere
3.1: N-ethyl-N,N-diisopropylamine; tetra-(n-butyl)ammonium iodide / 15 h / 20 °C
4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 14 h / 20 °C / Inert atmosphere
With
1H-imidazole; n-butyllithium; tetrabutyl ammonium fluoride; tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; hexane; N,N-dimethyl-formamide;
DOI:10.1039/c2cc33704e
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydride / hexane; mineral oil; 1-methyl-pyrrolidin-2-one / 1 h / 0 °C / Inert atmosphere
1.2: 4 h / 20 - 100 °C / Inert atmosphere
2.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / -78 °C / Inert atmosphere
2.2: 0.25 h / -78 °C / Inert atmosphere
3.1: N-ethyl-N,N-diisopropylamine; tetra-(n-butyl)ammonium iodide / 15 h / 20 °C
4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 14 h / 20 °C / Inert atmosphere
With
n-butyllithium; tetrabutyl ammonium fluoride; tetra-(n-butyl)ammonium iodide; sodium hydride; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; 1-methyl-pyrrolidin-2-one; hexane; mineral oil;
DOI:10.1039/c2cc33704e
