(2S,3R)-diphenylmethyl-3-<(benzyloxycarbonyl)oxy>-2-fluoro-tetradecanoate

Base Information

Chemical Name:(2S,3R)-diphenylmethyl-3-<(benzyloxycarbonyl)oxy>-2-fluoro-tetradecanoate
CAS No.:137344-84-4
Molecular Formula:C₃₅H₄₃FO₅
Molecular Weight:562.722
Hs Code.:

Synonyms:(2S,3R)-diphenylmethyl-3-<(benzyloxycarbonyl)oxy>-2-fluoro-tetradecanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3R)-diphenylmethyl-3-<(benzyloxycarbonyl)oxy>-2-fluoro-tetradecanoate

Chemical Property:

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Technology Process of (2S,3R)-diphenylmethyl-3-<(benzyloxycarbonyl)oxy>-2-fluoro-tetradecanoate

There total 2 articles about (2S,3R)-diphenylmethyl-3-<(benzyloxycarbonyl)oxy>-2-fluoro-tetradecanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 137344-83-3
(2S,3R)-diphenylmethyl-2-fluoro-3-hyroxytetradecanoate

: 501-53-1,94274-21-2
benzyl chloroformate

: 137344-84-4
(2S,3R)-diphenylmethyl-3-<(benzyloxycarbonyl)oxy>-2-fluoro-tetradecanoate

Guidance literature:: With dmap; In dichloromethane; 1) 30 min, 0 deg C, 2) 30 min, rt;
DOI:10.1016/S0040-4020(01)96156-3

Reference yield:

: 908093-98-1
diazodiphenylmethane

: 137344-84-4
(2S,3R)-diphenylmethyl-3-<(benzyloxycarbonyl)oxy>-2-fluoro-tetradecanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 900 mg / tetrahydrofuran / 5 h / 50 °C

2: 90 percent / DMAP / CH₂Cl₂ / 1) 30 min, 0 deg C, 2) 30 min, rt

With dmap; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4020(01)96156-3