C₄₁H₄₇N₃O₁₅

Base Information

Chemical Name:C₄₁H₄₇N₃O₁₅
CAS No.:1401413-75-9
Molecular Formula:C₄₁H₄₇N₃O₁₅
Molecular Weight:821.835
Hs Code.:

C<sub>41</sub>H<sub>47</sub>N<sub>3</sub>O<sub>15</sub>

Synonyms:C₄₁H₄₇N₃O₁₅

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₁H₄₇N₃O₁₅

Chemical Property:

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Technology Process of C₄₁H₄₇N₃O₁₅

There total 10 articles about C₄₁H₄₇N₃O₁₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1401413-68-0
C₂₇H₂₉N₃O₆

: 74808-10-9,86520-63-0,87119-53-7,92052-29-4,121238-27-5,142831-80-9,127061-80-7
2,3,4,6-tetra-O-acetyl-D-galactopyranosyl trichloroacetimidate

: 1401413-75-9
C₄₁H₄₇N₃O₁₅

Guidance literature:: C₂₇H₂₉N₃O₆; 2,3,4,6-tetra-O-acetyl-D-galactopyranosyl trichloroacetimidate; In dichloromethane; at 20 ℃; for 0.5h; Molecular sieve;

trifluorormethanesulfonic acid; In dichloromethane; at -70 - -20 ℃; for 1h;

Reference yield:

: 14131-63-6
D-glucosamine hydrochloride

: 1401413-75-9
C₄₁H₄₇N₃O₁₅

Guidance literature:: Multi-step reaction with 10 steps

1.1: sodium hydrogencarbonate / water / 0.5 h / 20 °C

1.2: 4.5 h / 20 °C

2.1: pyridine / 0 - 20 °C

3.1: boron trifluoride diethyl etherate / dichloromethane / 0 - 20 °C

4.1: zinc; acetic acid / dichloromethane; methanol / 1 h / 0 - 20 °C / Inert atmosphere

5.1: sodium methylate / dichloromethane; methanol / 2 h / 20 °C

5.2: pH ~ 7

6.1: potassium carbonate; triflic azide / zinc(II) chloride / dichloromethane; water; methanol / 20 °C

7.1: camphorsulfonic acid / toluene / 2 h / 20 °C

8.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 2 h / 0 - 20 °C

9.1: trifluorormethanesulfonic acid; triethylsilane / dichloromethane / 1 h / -78 °C

10.1: dichloromethane / 0.5 h / 20 °C / Molecular sieve

10.2: 1 h / -70 - -20 °C

With pyridine; triethylsilane; trifluorormethanesulfonic acid; triflic azide; boron trifluoride diethyl etherate; sodium methylate; sodium hydride; sodium hydrogencarbonate; potassium carbonate; acetic acid; zinc; zinc(II) chloride; In methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; mineral oil;

Reference yield:

: 122210-05-3
1,3,4,6-tetra-O-acetyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranose

: 1401413-75-9
C₄₁H₄₇N₃O₁₅

Guidance literature:: Multi-step reaction with 8 steps

1.1: boron trifluoride diethyl etherate / dichloromethane / 0 - 20 °C

2.1: zinc; acetic acid / dichloromethane; methanol / 1 h / 0 - 20 °C / Inert atmosphere

3.1: sodium methylate / dichloromethane; methanol / 2 h / 20 °C

3.2: pH ~ 7

4.1: potassium carbonate; triflic azide / zinc(II) chloride / dichloromethane; water; methanol / 20 °C

5.1: camphorsulfonic acid / toluene / 2 h / 20 °C

6.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 2 h / 0 - 20 °C

7.1: trifluorormethanesulfonic acid; triethylsilane / dichloromethane / 1 h / -78 °C

8.1: dichloromethane / 0.5 h / 20 °C / Molecular sieve

8.2: 1 h / -70 - -20 °C

With triethylsilane; trifluorormethanesulfonic acid; triflic azide; boron trifluoride diethyl etherate; sodium methylate; sodium hydride; potassium carbonate; acetic acid; zinc; zinc(II) chloride; In methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; mineral oil;