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Technology Process of 2B(C6H5)4(1-)*H3N(CH2)3OC6H4C6H4O(CH2)3NH3(2+)*(C5H5O(OH)(OCH3)2O)7={B(C6H5)4}2(C18H26N2O2)(C49H84O35)

2B(C6H5)4(1-)*H3N(CH2)3OC6H4C6H4O(CH2)3NH3(2+)*(C5H5O(OH)(OCH3)2O)7={B(C6H5)4}2(C18H26N2O2)(C49H84O35)

Base Information
  • Chemical Name:2B(C6H5)4(1-)*H3N(CH2)3OC6H4C6H4O(CH2)3NH3(2+)*(C5H5O(OH)(OCH3)2O)7={B(C6H5)4}2(C18H26N2O2)(C49H84O35)
  • CAS No.:124992-44-5
  • Molecular Formula:C18H26N2O2*2C24H20B*C49H84O35
  • Molecular Weight:2174.07
  • Hs Code.:
2B(C<sub>6</sub>H<sub>5</sub>)4<sup>(1-)</sup>*H<sub>3</sub>N(CH<sub>2</sub>)3OC<sub>6</sub>H<sub>4</sub>C<sub>6</sub>H<sub>4</sub>O(CH<sub>2</sub>)3NH<sub>3</sub><sup>(2+)</sup>*(C<sub>5</sub>H<sub>5</sub>O(OH)(OCH<sub>3</sub>)2O)7={B(C<sub>6</sub>H<sub>5</sub>)4}2(C<sub>18</sub>H<sub>26</sub>N<sub>2</sub>O<sub>2</sub>)(C<sub>49</sub>H<sub>84</sub>O<sub>35</sub>)

Synonyms:2B(C6H5)4(1-)*H3N(CH2)3OC6H4C6H4O(CH2)3NH3(2+)*(C5H5O(OH)(OCH3)2O)7={B(C6H5)4}2(C18H26N2O2)(C49H84O35)

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Chemical Property of 2B(C6H5)4(1-)*H3N(CH2)3OC6H4C6H4O(CH2)3NH3(2+)*(C5H5O(OH)(OCH3)2O)7={B(C6H5)4}2(C18H26N2O2)(C49H84O35)
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Technology Process of 2B(C6H5)4(1-)*H3N(CH2)3OC6H4C6H4O(CH2)3NH3(2+)*(C5H5O(OH)(OCH3)2O)7={B(C6H5)4}2(C18H26N2O2)(C49H84O35)

There total 1 articles about 2B(C6H5)4(1-)*H3N(CH2)3OC6H4C6H4O(CH2)3NH3(2+)*(C5H5O(OH)(OCH3)2O)7={B(C6H5)4}2(C18H26N2O2)(C49H84O35) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.2%

3,3'-(4,4'-biphenyldiyldioxy)bis(propylammonium)Cl<sub>2</sub>
124992-42-3

3,3'-(4,4'-biphenyldiyldioxy)bis(propylammonium)Cl2

heptakis(2,6-O-methyl)-β-cyclodextrin
51166-71-3

heptakis(2,6-O-methyl)-β-cyclodextrin

sodium tetraphenyl borate
143-66-8

sodium tetraphenyl borate

2B(C<sub>6</sub>H<sub>5</sub>)4<sup>(1-)</sup>*H<sub>3</sub>N(CH<sub>2</sub>)3OC<sub>6</sub>H<sub>4</sub>C<sub>6</sub>H<sub>4</sub>O(CH<sub>2</sub>)3NH<sub>3</sub><sup>(2+)</sup>*(C<sub>5</sub>H<sub>5</sub>O(OH)(OCH<sub>3</sub>)2O)7={B(C<sub>6</sub>H<sub>5</sub>)4}2(C<sub>18</sub>H<sub>26</sub>N<sub>2</sub>O<sub>2</sub>)(C<sub>49</sub>H<sub>84</sub>O<sub>35</sub>)
124992-44-5

2B(C6H5)4(1-)*H3N(CH2)3OC6H4C6H4O(CH2)3NH3(2+)*(C5H5O(OH)(OCH3)2O)7={B(C6H5)4}2(C18H26N2O2)(C49H84O35)

Guidance literature:
With sodium hydroxide; In water; Suspending of diammonium salt in H2O, addn. of Me-CD with viporous stirring, adjusting of pH wit aq. NaOH to 7, dropwise addn. of soln. of Na tetraphenylboron.; Centrifugation of white ppt., drying under high vac. overnight, elem. anal.;
DOI:10.1021/ja00165a054
upstream raw materials:

3,3'-(4,4'-biphenyldiyldioxy)bis(propylammonium)Cl2

heptakis(2,6-O-methyl)-β-cyclodextrin

sodium tetraphenyl borate

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