3-phenylthiocyclopentanol

Base Information

• Chemical Name: 3-phenylthiocyclopentanol
• CAS No.: 152584-31-1
• Molecular Formula: C₁₁H₁₄OS
• Molecular Weight: 194.298
• Mol file: 152584-31-1.mol

Synonyms:3-phenylthiocyclopentanol

Chemical Property of 3-phenylthiocyclopentanol

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 3-phenylthiocyclopentanol

There total 1 articles about 3-phenylthiocyclopentanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cyclopent-2-enone (930-30-3) + thiophenol (108-98-5) → 3-phenylthiocyclopentanol (152584-31-1)

Guidance literature:

With sodium tetrahydroborate; triethylamine; Yield given. Multistep reaction; 1.) chloroform, RT, 18 h, 2.) chloroform, ethanol, 10 min;

Reference yield: 88.0%

3-phenylthiocyclopentanol (152584-31-1) → 3-(phenylsulfonyl)cyclopentanol (67100-23-6)

Guidance literature:

With ammonium molybdate; dihydrogen peroxide; In methanol; at -10 ℃; for 16h;

Reference yield:

3-phenylthiocyclopentanol (152584-31-1) → 2-cyclopenten-1-yl phenyl sulfone (140396-96-9)

Guidance literature:

Multi-step reaction with 3 steps

1: 88 percent / ammonium molybdate, 27.5percent aq. H₂O₂ / methanol / 16 h / -10 °C

2: 78 percent / triethylamine / CH₂Cl₂ / 3 h / 0 °C

3: 93 percent / potassium tert-butoxide / 2-methyl-propan-2-ol / 28.5 °C

With ammonium molybdate; potassium tert-butylate; dihydrogen peroxide; triethylamine; In methanol; dichloromethane; tert-butyl alcohol;

upstream raw materials:

cyclopent-2-enone

thiophenol

Downstream raw materials:

3-(phenylsulfonyl)cyclopentanol

2-cyclopenten-1-yl phenyl sulfone

1-mesyloxy-3-phenylsulfonylcyclopentane