triphenylsulfonium 4-(3-(2-ethoxy-1,1-difluoro-2-oxoethoxy)adamantane-1-carbonyloxy)-1,1,2,2-tetrafluorobutane-1-sulfonate

Base Information

Chemical Name:triphenylsulfonium 4-(3-(2-ethoxy-1,1-difluoro-2-oxoethoxy)adamantane-1-carbonyloxy)-1,1,2,2-tetrafluorobutane-1-sulfonate
CAS No.:1335102-65-2
Molecular Formula:C₁₈H₁₅S*C₁₉H₂₃F₆O₈S
Molecular Weight:788.826
Hs Code.:

Synonyms:triphenylsulfonium 4-(3-(2-ethoxy-1,1-difluoro-2-oxoethoxy)adamantane-1-carbonyloxy)-1,1,2,2-tetrafluorobutane-1-sulfonate

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Chemical Property of triphenylsulfonium 4-(3-(2-ethoxy-1,1-difluoro-2-oxoethoxy)adamantane-1-carbonyloxy)-1,1,2,2-tetrafluorobutane-1-sulfonate

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Technology Process of triphenylsulfonium 4-(3-(2-ethoxy-1,1-difluoro-2-oxoethoxy)adamantane-1-carbonyloxy)-1,1,2,2-tetrafluorobutane-1-sulfonate

There total 7 articles about triphenylsulfonium 4-(3-(2-ethoxy-1,1-difluoro-2-oxoethoxy)adamantane-1-carbonyloxy)-1,1,2,2-tetrafluorobutane-1-sulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1335102-63-0
sodium 4-(3-(2-ethoxy-1,1-difluoro-2-oxoethoxy)adamantane-1-carbonyloxy)-1,1,2,2-tetrafluorobutane-1-sulfonate

: 3353-89-7
triphenylsulfonium bromide

: 1335102-65-2
triphenylsulfonium 4-(3-(2-ethoxy-1,1-difluoro-2-oxoethoxy)adamantane-1-carbonyloxy)-1,1,2,2-tetrafluorobutane-1-sulfonate

Guidance literature:: In dichloromethane; water; at 20 ℃; for 1h;

Reference yield:

: 4-bromo-3,3,4,4-tetrafluorobutyl 3-methoxymethoxyadamantane-1-carboxylate

: 1335102-65-2
triphenylsulfonium 4-(3-(2-ethoxy-1,1-difluoro-2-oxoethoxy)adamantane-1-carbonyloxy)-1,1,2,2-tetrafluorobutane-1-sulfonate

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium dithionite; sodium carbonate / dichloromethane; water / 3.58 h / 60 °C

2.1: sodium carbonate; sodium tungstate / water / 0.5 h

2.2: 3.5 h / 60 °C

3.1: sulfuric acid / dichloromethane; water / 1.33 h / 0 °C

4.1: potassium hydroxide / dichloromethane; water / 40 h / 40 °C

5.1: sulfuric acid / dichloromethane; water / 1 h / 40 °C

6.1: dichloromethane; water / 1 h / 20 °C

With sodium tungstate; sodium dithionite; sulfuric acid; sodium carbonate; potassium hydroxide; In dichloromethane; water;

Reference yield:

: 42711-75-1
3-hydroxyadamantane-1-carboxylic acid

: 1335102-65-2
triphenylsulfonium 4-(3-(2-ethoxy-1,1-difluoro-2-oxoethoxy)adamantane-1-carbonyloxy)-1,1,2,2-tetrafluorobutane-1-sulfonate

Guidance literature:: Multi-step reaction with 8 steps

1.1: N-ethyl-N,N-diisopropylamine / methanol; dichloromethane; water / 24 h / 20 °C

2.1: potassium tert-butylate / dichloromethane; dimethyl sulfoxide / 4 h / 60 °C

3.1: sodium dithionite; sodium carbonate / dichloromethane; water / 3.58 h / 60 °C

4.1: sodium carbonate; sodium tungstate / water / 0.5 h

4.2: 3.5 h / 60 °C

5.1: sulfuric acid / dichloromethane; water / 1.33 h / 0 °C

6.1: potassium hydroxide / dichloromethane; water / 40 h / 40 °C

7.1: sulfuric acid / dichloromethane; water / 1 h / 40 °C

8.1: dichloromethane; water / 1 h / 20 °C

With sodium tungstate; sodium dithionite; sulfuric acid; potassium tert-butylate; sodium carbonate; N-ethyl-N,N-diisopropylamine; potassium hydroxide; In methanol; dichloromethane; water; dimethyl sulfoxide;