tricarbonyl(3-oxo-2-phenylspiro{2-azabicyclo{3.3.0}octane-4,1'-{2,4}-cyclohexadiene})iron

Base Information

Chemical Name:tricarbonyl(3-oxo-2-phenylspiro{2-azabicyclo{3.3.0}octane-4,1'-{2,4}-cyclohexadiene})iron
CAS No.:120474-98-8
Molecular Formula:C₂₁H₁₉FeNO₄
Molecular Weight:405.233
Hs Code.:

Synonyms:tricarbonyl(3-oxo-2-phenylspiro{2-azabicyclo{3.3.0}octane-4,1'-{2,4}-cyclohexadiene})iron

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Chemical Property of tricarbonyl(3-oxo-2-phenylspiro{2-azabicyclo{3.3.0}octane-4,1'-{2,4}-cyclohexadiene})iron

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Technology Process of tricarbonyl(3-oxo-2-phenylspiro{2-azabicyclo{3.3.0}octane-4,1'-{2,4}-cyclohexadiene})iron

There total 1 articles about tricarbonyl(3-oxo-2-phenylspiro{2-azabicyclo{3.3.0}octane-4,1'-{2,4}-cyclohexadiene})iron which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 120474-88-6,120574-06-3
tricarbonyl(N-cyclopent-2-en-1-yl-N-phenyl-1-4-η-cyclohexa-1,3-dienecarboxylate)iron

: 120474-98-8
tricarbonyl(3-oxo-2-phenylspiro{2-azabicyclo{3.3.0}octane-4,1'-{2,4}-cyclohexadiene})iron

Guidance literature:: With carbon monoxide; In further solvent(s); Bu2O-soln. of N-allyl amide purged with CO for 1 min, refluxed for 6 h; cooled to room temp.; diluted (Et2O), filtered, concd.; TCL (20% EtOAc/hex); yielded an epimeric mixt. (1:1);
DOI:10.1021/ja00193a023