N-(4-Methoxyphenyl)-3-methyl-2-(4-nitrobenzyl)-4-phenyl-3-isothiazolin-5-imin

Base Information

Chemical Name:N-(4-Methoxyphenyl)-3-methyl-2-(4-nitrobenzyl)-4-phenyl-3-isothiazolin-5-imin
CAS No.:77596-40-8
Molecular Formula:C₂₄H₂₁N₃O₃S
Molecular Weight:431.515
Hs Code.:

Synonyms:N-(4-Methoxyphenyl)-3-methyl-2-(4-nitrobenzyl)-4-phenyl-3-isothiazolin-5-imin

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Chemical Property of N-(4-Methoxyphenyl)-3-methyl-2-(4-nitrobenzyl)-4-phenyl-3-isothiazolin-5-imin

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Technology Process of N-(4-Methoxyphenyl)-3-methyl-2-(4-nitrobenzyl)-4-phenyl-3-isothiazolin-5-imin

There total 3 articles about N-(4-Methoxyphenyl)-3-methyl-2-(4-nitrobenzyl)-4-phenyl-3-isothiazolin-5-imin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 77596-21-5
N-(4-Methoxyphenyl)-3-(4-nitrobenzylamino)-2-phenylcrotonthioamid

: 77596-40-8
N-(4-Methoxyphenyl)-3-methyl-2-(4-nitrobenzyl)-4-phenyl-3-isothiazolin-5-imin

Guidance literature:: With pyridine; bromine; In ethyl acetate; at 0 - 10 ℃;

Reference yield:

: 18600-42-5
4-nitrobenzylamine hydrochloride

: 77596-40-8
N-(4-Methoxyphenyl)-3-methyl-2-(4-nitrobenzyl)-4-phenyl-3-isothiazolin-5-imin

Guidance literature:: Multi-step reaction with 2 steps

1: 1) N(C₂H₅)3, 2) H₂O / 1) ethanol, 24 h, 2) ethanol, 0 deg C

2: 57 percent / Br₂, pyridine / ethyl acetate / 0 - 10 °C

With pyridine; water; bromine; triethylamine; In ethyl acetate;

Reference yield:

: 75184-18-8
N-(4-Methoxyphenyl)-3-oxo-2-(phenyl)thiobuttersaeure-amid

: 77596-40-8
N-(4-Methoxyphenyl)-3-methyl-2-(4-nitrobenzyl)-4-phenyl-3-isothiazolin-5-imin

Guidance literature:: Multi-step reaction with 2 steps

1: 1) N(C₂H₅)3, 2) H₂O / 1) ethanol, 24 h, 2) ethanol, 0 deg C

2: 57 percent / Br₂, pyridine / ethyl acetate / 0 - 10 °C

With pyridine; water; bromine; triethylamine; In ethyl acetate;