2-(1H-benzo[d]imidazol-1-yl)-N-p-tolylaniline

Base Information

Chemical Name:2-(1H-benzo[d]imidazol-1-yl)-N-p-tolylaniline
CAS No.:1352820-62-2
Molecular Formula:C₂₀H₁₇N₃
Molecular Weight:299.375
Hs Code.:

Synonyms:2-(1H-benzo[d]imidazol-1-yl)-N-p-tolylaniline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(1H-benzo[d]imidazol-1-yl)-N-p-tolylaniline

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Technology Process of 2-(1H-benzo[d]imidazol-1-yl)-N-p-tolylaniline

There total 4 articles about 2-(1H-benzo[d]imidazol-1-yl)-N-p-tolylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 26268-23-5
2‐(1H‐benzo[d]imidazol‐1‐yl)aniline

: 624-31-7
4-tolyl iodide

: 1352820-62-2
2-(1H-benzo[d]imidazol-1-yl)-N-p-tolylaniline

Guidance literature:: With potassium phosphate; copper(l) iodide; In tetrahydrofuran; at 110 ℃; for 24h; Inert atmosphere;
DOI:10.1021/ol202884z

Reference yield:

: 51-17-2,79351-71-6
benzoimidazole

: 1352820-62-2
2-(1H-benzo[d]imidazol-1-yl)-N-p-tolylaniline

Guidance literature:: Multi-step reaction with 3 steps

1: copper(l) iodide; potassium carbonate / N,N-dimethyl-formamide / 24 h / 110 °C / Inert atmosphere

2: palladium 10% on activated carbon; hydrogen / ethanol / 4 h / 20 °C / 2280.15 Torr

3: copper(l) iodide; potassium phosphate / tetrahydrofuran / 24 h / 110 °C / Inert atmosphere

With potassium phosphate; copper(l) iodide; palladium 10% on activated carbon; hydrogen; potassium carbonate; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/ol202884z

Reference yield:

: 25688-28-2
1‐(2‐nitrophenyl)‐1H‐benzo[d]imidazole

: 1352820-62-2
2-(1H-benzo[d]imidazol-1-yl)-N-p-tolylaniline

Guidance literature:: Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen / ethanol / 4 h / 20 °C / 2280.15 Torr

2: copper(l) iodide; potassium phosphate / tetrahydrofuran / 24 h / 110 °C / Inert atmosphere

With potassium phosphate; copper(l) iodide; palladium 10% on activated carbon; hydrogen; In tetrahydrofuran; ethanol;
DOI:10.1021/ol202884z