C₃₃H₄₅NO₃Si

Base Information

Chemical Name:C₃₃H₄₅NO₃Si
CAS No.:1450843-31-8
Molecular Formula:C₃₃H₄₅NO₃Si
Molecular Weight:531.811
Hs Code.:

C<sub>33</sub>H<sub>45</sub>NO<sub>3</sub>Si

Synonyms:C₃₃H₄₅NO₃Si

Suppliers and Price of C₃₃H₄₅NO₃Si

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₃H₄₅NO₃Si

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₃H₄₅NO₃Si

There total 2 articles about C₃₃H₄₅NO₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1262034-08-1
tert-butyl 2-(3-methoxyprop-1-ynyl)phenylcarbamate

: 162109-81-1
C₁₉H₃₀OSi

: 1450843-31-8
C₃₃H₄₅NO₃Si

Guidance literature:: With Zeise's dimer; tris(pentafluorophenyl)phosphine; In 1,4-dioxane; at 20 ℃; for 1h; Molecular sieve;
DOI:10.1055/s-0033-1338938

Reference yield:

: 161117-84-6
tert-butyl 2-iodophenylcarbamate

: 1450843-31-8
C₃₃H₄₅NO₃Si

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) iodide; triethylamine; bis-triphenylphosphine-palladium(II) chloride / 2 h / 20 °C / Inert atmosphere

2: di(rhodium)tetracarbonyl dichloride; tris(1,1,1,3,3,3-hexafluoroisopropyl)phosphite; sodium carbonate / 1,4-dioxane / 12 h / 100 °C / Inert atmosphere; Sealed tube

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; di(rhodium)tetracarbonyl dichloride; tris(1,1,1,3,3,3-hexafluoroisopropyl)phosphite; sodium carbonate; triethylamine; In 1,4-dioxane;
DOI:10.1002/anie.201209266