4-FLUORO-3-METHOXYANILINE HYDROCHLORIDE 98

Base Information

• Chemical Name: 4-FLUORO-3-METHOXYANILINE HYDROCHLORIDE 98
• CAS No.: 22510-10-7
• Molecular Formula: C7H8 F N O . Cl H
• Molecular Weight: 177.606
• Hs Code.: 2922299090
• Mol file: 22510-10-7.mol

Synonyms:Benzenamine,4-fluoro-3-methoxy-, hydrochloride (9CI); m-Anisidine, 4-fluoro-, hydrochloride(8CI); 4-Fluoro-3-methoxyaniline hydrochloride

Chemical Property of 4-FLUORO-3-METHOXYANILINE HYDROCHLORIDE 98

Chemical Property:

• Vapor Pressure: 0.00203mmHg at 25°C
• Melting Point: 248-250
• Boiling Point: 286.3°Cat760mmHg
• Flash Point: 127°C
• PSA: 35.25000
• Density: g/cm³
• LogP: 2.79970
• Storage Temp.: Keep Cold

Purity/Quality:

97% ^*data from raw suppliers

4-Fluoro-3-methoxyanilinehydrochloride ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 4-Fluoro-3-methoxyaniline, HCl

Technology Process of 4-FLUORO-3-METHOXYANILINE HYDROCHLORIDE 98

There total 1 articles about 4-FLUORO-3-METHOXYANILINE HYDROCHLORIDE 98 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

(tert-butoxy)-N-(4-fluoro-3-methoxyphenyl)carboxamide (774232-94-9) → 4-fluoro-3-methoxyphenylamine hydrochloride (22510-10-7)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; at 20 ℃;

Reference yield: 63.0%

4-fluoro-3-methoxyphenylamine hydrochloride (22510-10-7) + 1-[cis-3,5-bis-(tert-butyl-diphenyl-silanyloxy)-cyclohexyl]-7-chloro-3-(2-fluoro-4-methoxy-phenyl)-3,4-dihydro-1H-pyrimido[4,5-d]pyrimidin-2-one → 1-[cis-3,5-bis-(tert-butyl-diphenyl-silanyloxy)-cyclohexyl]-3-(2-fluoro-4-methoxy-phenyl)-7-(4-fluoro-3-methoxy-phenylamino)-3,4-dihydro-1H-pyrimido[4,5-d]pyrimidin-2-one

Guidance literature:

In isopropyl alcohol; at 160 ℃; for 0.166667h; Microwave SmithSynthesizer;

Reference yield:

4-fluoro-3-methoxyphenylamine hydrochloride (22510-10-7) + 1-[cis-3,5-bis-(tert-butyl-diphenyl-silanyloxy)-cyclohexyl]-7-chloro-3-(4-methoxy-phenyl)-3,4-dihydro-1H-pyrimido[4,5-d]pyrimidin-2-one → 1-[cis-3,5-bis-(tert-butyl-diphenyl-silanyloxy)-cyclohexyl]-3-(4-methoxy-phenyl)-7-(4-fluoro-3-methoxy-phenylamino)-3,4-dihydro-1H-pyrimido[4,5-d]pyrimidin-2-one

Guidance literature:

In isopropyl alcohol; at 160 ℃; for 0.166667h; Microwave SmithSynthesizer;

upstream raw materials:

(tert-butoxy)-N-(4-fluoro-3-methoxyphenyl)carboxamide

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