(2R,3R)-(+)-2-carbomethoxy-3-carboxanilide-1,4,7,10,13,16-hexaoxacyclooctadecane

Base Information

Chemical Name:(2R,3R)-(+)-2-carbomethoxy-3-carboxanilide-1,4,7,10,13,16-hexaoxacyclooctadecane
CAS No.:111216-15-0
Molecular Formula:C₂₁H₃₁NO₉
Molecular Weight:441.478
Hs Code.:

Synonyms:(2R,3R)-(+)-2-carbomethoxy-3-carboxanilide-1,4,7,10,13,16-hexaoxacyclooctadecane

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Chemical Property of (2R,3R)-(+)-2-carbomethoxy-3-carboxanilide-1,4,7,10,13,16-hexaoxacyclooctadecane

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Technology Process of (2R,3R)-(+)-2-carbomethoxy-3-carboxanilide-1,4,7,10,13,16-hexaoxacyclooctadecane

There total 3 articles about (2R,3R)-(+)-2-carbomethoxy-3-carboxanilide-1,4,7,10,13,16-hexaoxacyclooctadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: (2R,3R)-3-Phenylcarbamoyl-1,4,7,10,13,16-hexaoxa-cyclooctadecane-2-carboxylic acid

: 111216-15-0
(2R,3R)-(+)-2-carbomethoxy-3-carboxanilide-1,4,7,10,13,16-hexaoxacyclooctadecane

Guidance literature:: In tetrahydrofuran; diethyl ether; at 0 ℃;

Reference yield:

: 76871-58-4
(R,R)-1,4,7,10,13,16-Hexaoxacyclooctadecane-2,3-dicarboxylic acid anhydride

: 111216-15-0
(2R,3R)-(+)-2-carbomethoxy-3-carboxanilide-1,4,7,10,13,16-hexaoxacyclooctadecane

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / CH₂Cl₂ / 2 h / Ambient temperature

2: 96 percent / tetrahydrofuran; diethyl ether / 0 °C

In tetrahydrofuran; diethyl ether; dichloromethane;

Reference yield:

: 62-53-3
aniline

: 111216-15-0
(2R,3R)-(+)-2-carbomethoxy-3-carboxanilide-1,4,7,10,13,16-hexaoxacyclooctadecane

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / CH₂Cl₂ / 2 h / Ambient temperature

2: 96 percent / tetrahydrofuran; diethyl ether / 0 °C

In tetrahydrofuran; diethyl ether; dichloromethane;