N,N',N''-(2,4,6-triethylbenzene-1,3,5-triyl)tris(methylene)tris(2,2,2-trifluoroacetamide)

Base Information

Chemical Name:N,N',N''-(2,4,6-triethylbenzene-1,3,5-triyl)tris(methylene)tris(2,2,2-trifluoroacetamide)
CAS No.:1137672-92-4
Molecular Formula:C₂₁H₂₄F₉N₃O₃
Molecular Weight:537.425
Hs Code.:

Synonyms:N,N',N''-(2,4,6-triethylbenzene-1,3,5-triyl)tris(methylene)tris(2,2,2-trifluoroacetamide)

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Chemical Property of N,N',N''-(2,4,6-triethylbenzene-1,3,5-triyl)tris(methylene)tris(2,2,2-trifluoroacetamide)

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Technology Process of N,N',N''-(2,4,6-triethylbenzene-1,3,5-triyl)tris(methylene)tris(2,2,2-trifluoroacetamide)

There total 2 articles about N,N',N''-(2,4,6-triethylbenzene-1,3,5-triyl)tris(methylene)tris(2,2,2-trifluoroacetamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 354-38-1
2,2,2-trifluoroacetamide

: 181058-08-2
1,3,5-tris(bromomethyl)-2,4,6-triethylbenzene

: 1137672-92-4
N,N',N''-(2,4,6-triethylbenzene-1,3,5-triyl)tris(methylene)tris(2,2,2-trifluoroacetamide)

Guidance literature:: 2,2,2-trifluoroacetamide; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; Cooling with ice; Inert atmosphere;

1,3,5-tris(bromomethyl)-2,4,6-triethylbenzene; In N,N-dimethyl-formamide; at 20 ℃; for 0.18h; Inert atmosphere;

Reference yield: 28.0%

: 407-25-0
trifluoroacetic anhydride

: 149525-65-5
1,3,5-triethyl-2,4,6-tris(aminomethyl)benzene

: 1137672-92-4
N,N',N''-(2,4,6-triethylbenzene-1,3,5-triyl)tris(methylene)tris(2,2,2-trifluoroacetamide)

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 60 ℃; for 24h; Inert atmosphere;
DOI:10.1021/jo9000788

Reference yield: 96.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 1137672-92-4
N,N',N''-(2,4,6-triethylbenzene-1,3,5-triyl)tris(methylene)tris(2,2,2-trifluoroacetamide)

: [3,5-bis-(tert-butoxycarbonylamino-methyl)-2,4,6-triethyl-benzyl]-carbamic acid tert-butyl ester

Guidance literature:: N,N',N''-(2,4,6-triethylbenzene-1,3,5-triyl)tris(methylene)tris(2,2,2-trifluoroacetamide); With sodium hydroxide; In methanol; water; at 65 ℃; for 18h;

di-tert-butyl dicarbonate; With triethylamine; In methanol; water; at 20 ℃; for 4h;