methyl (2R,5R,8S)-2-allyl-8-(4-allyloxybenzyl)-3,6,9-triaza-5-(3-[N'-{2,2,5,7,8-pentamethyl-3,4-dihydro-2H-chromen-6-ylsulfonyl}guanidino]propyl)-4,7,10-trioxoundecanoate

Base Information

Chemical Name:methyl (2R,5R,8S)-2-allyl-8-(4-allyloxybenzyl)-3,6,9-triaza-5-(3-[N'-{2,2,5,7,8-pentamethyl-3,4-dihydro-2H-chromen-6-ylsulfonyl}guanidino]propyl)-4,7,10-trioxoundecanoate
CAS No.:900522-13-6
Molecular Formula:C₄₀H₅₆N₆O₉S
Molecular Weight:796.985
Hs Code.:

methyl (2R,5R,8S)-2-allyl-8-(4-allyloxybenzyl)-3,6,9-triaza-5-(3-[N'-{2,2,5,7,8-pentamethyl-3,4-dihydro-2H-chromen-6-ylsulfonyl}guanidino]propyl)-4,7,10-trioxoundecanoate

Synonyms:methyl (2R,5R,8S)-2-allyl-8-(4-allyloxybenzyl)-3,6,9-triaza-5-(3-[N'-{2,2,5,7,8-pentamethyl-3,4-dihydro-2H-chromen-6-ylsulfonyl}guanidino]propyl)-4,7,10-trioxoundecanoate

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Chemical Property of methyl (2R,5R,8S)-2-allyl-8-(4-allyloxybenzyl)-3,6,9-triaza-5-(3-[N'-{2,2,5,7,8-pentamethyl-3,4-dihydro-2H-chromen-6-ylsulfonyl}guanidino]propyl)-4,7,10-trioxoundecanoate

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Technology Process of methyl (2R,5R,8S)-2-allyl-8-(4-allyloxybenzyl)-3,6,9-triaza-5-(3-[N'-{2,2,5,7,8-pentamethyl-3,4-dihydro-2H-chromen-6-ylsulfonyl}guanidino]propyl)-4,7,10-trioxoundecanoate

There total 2 articles about methyl (2R,5R,8S)-2-allyl-8-(4-allyloxybenzyl)-3,6,9-triaza-5-(3-[N'-{2,2,5,7,8-pentamethyl-3,4-dihydro-2H-chromen-6-ylsulfonyl}guanidino]propyl)-4,7,10-trioxoundecanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 900522-12-5
methyl (2R,5R)-2-allyl-5-amino-3-aza-8-[N'-(2,2,5,7,8-pentamethyl-3,4-dihydro-2H-chromen-6-ylsulfonyl)guanidino]-4-oxooctanoate

: 171813-89-1
(2S)-2-acetamido-3-(4-allyloxyphenyl)propanoic acid

: 900522-13-6
methyl (2R,5R,8S)-2-allyl-8-(4-allyloxybenzyl)-3,6,9-triaza-5-(3-[N'-{2,2,5,7,8-pentamethyl-3,4-dihydro-2H-chromen-6-ylsulfonyl}guanidino]propyl)-4,7,10-trioxoundecanoate

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 16h;
DOI:10.1016/j.tet.2008.09.031

Reference yield: 64.0%

: 900522-13-6
methyl (2R,5R,8S)-2-allyl-8-(4-allyloxybenzyl)-3,6,9-triaza-5-(3-[N'-{2,2,5,7,8-pentamethyl-3,4-dihydro-2H-chromen-6-ylsulfonyl}guanidino]propyl)-4,7,10-trioxoundecanoate

Guidance literature:

Reference yield: 100.0%

: 900522-13-6
methyl (2R,5R,8S)-2-allyl-8-(4-allyloxybenzyl)-3,6,9-triaza-5-(3-[N'-{2,2,5,7,8-pentamethyl-3,4-dihydro-2H-chromen-6-ylsulfonyl}guanidino]propyl)-4,7,10-trioxoundecanoate

: 900521-49-5
methyl (2R,5R,8S)-2-allyl-8-(4-allyloxybenzyl)-3,6,9-triaza-5-(3-[guanidino]propyl)-4,7,10-trioxoundecanoate hydrochloride

Guidance literature:: methyl (2R,5R,8S)-2-allyl-8-(4-allyloxybenzyl)-3,6,9-triaza-5-(3-[N'-{2,2,5,7,8-pentamethyl-3,4-dihydro-2H-chromen-6-ylsulfonyl}guanidino]propyl)-4,7,10-trioxoundecanoate; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 3h;

With hydrogenchloride; In methanol; diethyl ether; water;
DOI:10.1016/j.tet.2008.09.031