4,4'-bis[4-(2,2':6',2'’-terpyridinyl)]phenyltriphenylamine

Base Information

Chemical Name:4,4'-bis[4-(2,2':6',2'’-terpyridinyl)]phenyltriphenylamine
CAS No.:1384597-64-1
Molecular Formula:C₆₀H₄₁N₇
Molecular Weight:860.032
Hs Code.:

Synonyms:4,4'-bis[4-(2,2':6',2'’-terpyridinyl)]phenyltriphenylamine

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Chemical Property of 4,4'-bis[4-(2,2':6',2'’-terpyridinyl)]phenyltriphenylamine

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Technology Process of 4,4'-bis[4-(2,2':6',2'’-terpyridinyl)]phenyltriphenylamine

There total 6 articles about 4,4'-bis[4-(2,2':6',2'’-terpyridinyl)]phenyltriphenylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.9%

: 267221-89-6
N-phenyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-N-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]aniline

: 89972-76-9
4'-(4-bromo-phenyl)-[2,2';6',2'']terpyridine

: 1384597-64-1
4,4'-bis[4-(2,2':6',2'’-terpyridinyl)]phenyltriphenylamine

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In tetrahydrofuran; water; at 70 ℃; for 15h;
DOI:10.1016/j.dyepig.2012.05.004

Reference yield:

: 1122-62-9
2-acetylpyridine

: 1384597-64-1
4,4'-bis[4-(2,2':6',2'’-terpyridinyl)]phenyltriphenylamine

Guidance literature:: Multi-step reaction with 3 steps

1.1: iodine / 0.5 h / 70 °C

1.2: 4 h / 80 °C

2.1: ammonium acetate / methanol / 70 °C

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / tetrahydrofuran; water / 15 h / 70 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; ammonium acetate; iodine; sodium carbonate; In tetrahydrofuran; methanol; water;
DOI:10.1016/j.dyepig.2012.05.004

Reference yield:

: 1122-91-4
4-bromo-benzaldehyde

: 1384597-64-1
4,4'-bis[4-(2,2':6',2'’-terpyridinyl)]phenyltriphenylamine

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / methanol; water / 2 h / 20 °C

2: ammonium acetate / methanol / 70 °C

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / tetrahydrofuran; water / 15 h / 70 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; ammonium acetate; sodium carbonate; sodium hydroxide; In tetrahydrofuran; methanol; water;
DOI:10.1016/j.dyepig.2012.05.004