P-(triethylammonio)-N⁶-benzoyl-5'-O-adenylyl-3'<*>5'-N⁴-benzoyl-2',3'-di-O-benzoylcytidine

Base Information

• Chemical Name: P-(triethylammonio)-N⁶-benzoyl-5'-O-adenylyl-3'<*>5'-N⁴-benzoyl-2',3'-di-O-benzoylcytidine
• CAS No.: 111772-30-6
• Molecular Formula: C₆H₁₅N*C₅₅H₄₅Br₂N₈O₁₆P
• Molecular Weight: 1365.98

Synonyms:P-(triethylammonio)-N⁶-benzoyl-5'-O-adenylyl-3'<*>5'-N⁴-benzoyl-2',3'-di-O-benzoylcytidine

Chemical Property of P-(triethylammonio)-N⁶-benzoyl-5'-O-adenylyl-3'<*>5'-N⁴-benzoyl-2',3'-di-O-benzoylcytidine

Chemical Property:

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Technology Process of P-(triethylammonio)-N⁶-benzoyl-5'-O-adenylyl-3'<*>5'-N⁴-benzoyl-2',3'-di-O-benzoylcytidine

There total 1 articles about P-(triethylammonio)-N⁶-benzoyl-5'-O-adenylyl-3'<*>5'-N⁴-benzoyl-2',3'-di-O-benzoylcytidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

P-(triethylammonio)-N6-benzoyl-2'-O-(4-methoxytetrahydropyran-4-yl)-5'-O-adenylyl-3'<*>5'-N4-benzoyl-2',3'-di-O-benzoylcytidine (111772-29-3) → P-(triethylammonio)-N6-benzoyl-5'-O-adenylyl-3'<*>5'-N4-benzoyl-2',3'-di-O-benzoylcytidine (111772-30-6)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; water; for 3h; Ambient temperature;

DOI:10.1021/jo00238a006

Reference yield:

5'-O-<(diisopropylamino)methoxyphosphino>-2',3'-O-(methoxymethylene)-O6-(diphenylcarbamoyl)-N2-propionylguanosine (109606-22-6) + P-(triethylammonio)-N6-benzoyl-5'-O-adenylyl-3'<*>5'-N4-benzoyl-2',3'-di-O-benzoylcytidine (111772-30-6) → C84H74Br2N14O26P2*C6H15N (111772-31-7)

Guidance literature:

With 1H-tetrazole; iodine; Yield given. Multistep reaction; 1.) acetonitrile, RT, 1 h, 2.) THF, lutidine, H₂O, 5 min;

DOI:10.1021/jo00238a006

upstream raw materials:

P-(triethylammonio)-N⁶-benzoyl-2'-O-(4-methoxytetrahydropyran-4-yl)-5'-O-adenylyl-3'<*>5'-N⁴-benzoyl-2',3'-di-O-benzoylcytidine

Downstream raw materials:

C₈₄H₇₄Br₂N₁₄O₂₆P₂*C₆H₁₅N

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