(E)-N-(1-(2-cinnamyl-4,5-dimethoxyphenyl)propan-2-yl)benzenesulfonamide

Base Information

Chemical Name:(E)-N-(1-(2-cinnamyl-4,5-dimethoxyphenyl)propan-2-yl)benzenesulfonamide
CAS No.:1414943-11-5
Molecular Formula:C₂₆H₂₉NO₄S
Molecular Weight:451.587
Hs Code.:

Synonyms:(E)-N-(1-(2-cinnamyl-4,5-dimethoxyphenyl)propan-2-yl)benzenesulfonamide

Suppliers and Price of (E)-N-(1-(2-cinnamyl-4,5-dimethoxyphenyl)propan-2-yl)benzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-N-(1-(2-cinnamyl-4,5-dimethoxyphenyl)propan-2-yl)benzenesulfonamide

Chemical Property:

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Technology Process of (E)-N-(1-(2-cinnamyl-4,5-dimethoxyphenyl)propan-2-yl)benzenesulfonamide

There total 1 articles about (E)-N-(1-(2-cinnamyl-4,5-dimethoxyphenyl)propan-2-yl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 812646-66-5
2-(but-2-enyl)-4,5-dimethoxybenzaldehyde

: 1414943-11-5
(E)-N-(1-(2-cinnamyl-4,5-dimethoxyphenyl)propan-2-yl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: ammonium acetate / Reflux; Inert atmosphere

2: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 20 °C / Cooling with ice

3: potassium carbonate / dichloromethane / 4 h / 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; ammonium acetate; potassium carbonate; In tetrahydrofuran; dichloromethane; 1: |Henry Nitro Aldol Condensation;
DOI:10.1016/j.tet.2012.10.017

Reference yield: 62.0%

: 1414943-11-5
(E)-N-(1-(2-cinnamyl-4,5-dimethoxyphenyl)propan-2-yl)benzenesulfonamide

: 1414943-18-2
3-benzenesulfonyl-7,8-dimethoxy-2-methyl-2,3-dihydro-1H-benzo[d]azepine

Guidance literature:: (E)-N-(1-(2-cinnamyl-4,5-dimethoxyphenyl)propan-2-yl)benzenesulfonamide; With osmium(VIII) oxide; 4-methylmorpholine N-oxide; In tetrahydrofuran; water; at 20 ℃; for 2h; Inert atmosphere;

With sodium periodate; In tetrahydrofuran; water; at 20 ℃; for 1h; Inert atmosphere;

With acetic acid; In tetrahydrofuran; water; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1016/j.tet.2012.10.017

Reference yield:

: 1414943-11-5
(E)-N-(1-(2-cinnamyl-4,5-dimethoxyphenyl)propan-2-yl)benzenesulfonamide

: 1414942-96-3
7,8-dimethoxy-2-methyl-3-phenylsulfonyl-2,3,4,5-tetrahydro-1H-benzo[d]azepine

Guidance literature:: Multi-step reaction with 2 steps

1.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tetrahydrofuran; water / 2 h / 20 °C / Inert atmosphere

1.2: 1 h / 20 °C / Inert atmosphere

1.3: 1 h / 20 °C / Inert atmosphere

2.1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 2.17 h / 20 °C / Inert atmosphere

With osmium(VIII) oxide; palladium 10% on activated carbon; hydrogen; 4-methylmorpholine N-oxide; In tetrahydrofuran; water; ethyl acetate;
DOI:10.1016/j.tet.2012.10.017