2-(2-(2-(4-(2-(benzyloxycarbonylamino)ethyl)-2-(2,2-dimethyl-4-oxo-3,8,11-trioxa-5-azatridecan-13-yloxy)phenoxy)ethoxy)ethoxy)ethyl tert-butylcarbamate

Base Information

Chemical Name:2-(2-(2-(4-(2-(benzyloxycarbonylamino)ethyl)-2-(2,2-dimethyl-4-oxo-3,8,11-trioxa-5-azatridecan-13-yloxy)phenoxy)ethoxy)ethoxy)ethyl tert-butylcarbamate
CAS No.:1400565-52-7
Molecular Formula:C₃₈H₅₉N₃O₁₂
Molecular Weight:749.899
Hs Code.:

2-(2-(2-(4-(2-(benzyloxycarbonylamino)ethyl)-2-(2,2-dimethyl-4-oxo-3,8,11-trioxa-5-azatridecan-13-yloxy)phenoxy)ethoxy)ethoxy)ethyl tert-butylcarbamate

Synonyms:2-(2-(2-(4-(2-(benzyloxycarbonylamino)ethyl)-2-(2,2-dimethyl-4-oxo-3,8,11-trioxa-5-azatridecan-13-yloxy)phenoxy)ethoxy)ethoxy)ethyl tert-butylcarbamate

Suppliers and Price of 2-(2-(2-(4-(2-(benzyloxycarbonylamino)ethyl)-2-(2,2-dimethyl-4-oxo-3,8,11-trioxa-5-azatridecan-13-yloxy)phenoxy)ethoxy)ethoxy)ethyl tert-butylcarbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-(2-(2-(4-(2-(benzyloxycarbonylamino)ethyl)-2-(2,2-dimethyl-4-oxo-3,8,11-trioxa-5-azatridecan-13-yloxy)phenoxy)ethoxy)ethoxy)ethyl tert-butylcarbamate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-(2-(2-(4-(2-(benzyloxycarbonylamino)ethyl)-2-(2,2-dimethyl-4-oxo-3,8,11-trioxa-5-azatridecan-13-yloxy)phenoxy)ethoxy)ethoxy)ethyl tert-butylcarbamate

There total 4 articles about 2-(2-(2-(4-(2-(benzyloxycarbonylamino)ethyl)-2-(2,2-dimethyl-4-oxo-3,8,11-trioxa-5-azatridecan-13-yloxy)phenoxy)ethoxy)ethoxy)ethyl tert-butylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 206265-94-3
2,2-dimethyl-4-oxo-3,8,11-trioxa-5-azatridecane-13-yl 4-methylbenzenesulfonate

: 37034-22-3
N-benzyloxycarbonyl-3,4-dihydroxyphenylethylamine

: 1400565-52-7
2-(2-(2-(4-(2-(benzyloxycarbonylamino)ethyl)-2-(2,2-dimethyl-4-oxo-3,8,11-trioxa-5-azatridecan-13-yloxy)phenoxy)ethoxy)ethoxy)ethyl tert-butylcarbamate

Guidance literature:: N-benzyloxycarbonyl-3,4-dihydroxyphenylethylamine; With caesium carbonate; In methanol; at 45 ℃; for 0.5h; Inert atmosphere;

2,2-dimethyl-4-oxo-3,8,11-trioxa-5-azatridecane-13-yl 4-methylbenzenesulfonate; In N,N-dimethyl-formamide; at 60 ℃; Inert atmosphere;
DOI:10.1055/s-0031-1290444

Reference yield:

: 51-61-6
dopamine

: 1400565-52-7
2-(2-(2-(4-(2-(benzyloxycarbonylamino)ethyl)-2-(2,2-dimethyl-4-oxo-3,8,11-trioxa-5-azatridecan-13-yloxy)phenoxy)ethoxy)ethoxy)ethyl tert-butylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium carbonate / diethyl ether; water / 3 h / 0 - 20 °C

2.1: caesium carbonate / methanol / 0.5 h / 45 °C / Inert atmosphere

2.2: 60 °C / Inert atmosphere

With sodium carbonate; caesium carbonate; In methanol; diethyl ether; water;
DOI:10.1055/s-0031-1290444

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 1400565-52-7
2-(2-(2-(4-(2-(benzyloxycarbonylamino)ethyl)-2-(2,2-dimethyl-4-oxo-3,8,11-trioxa-5-azatridecan-13-yloxy)phenoxy)ethoxy)ethoxy)ethyl tert-butylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium carbonate / diethyl ether; water / 3 h / 0 - 20 °C

2.1: caesium carbonate / methanol / 0.5 h / 45 °C / Inert atmosphere

2.2: 60 °C / Inert atmosphere

With sodium carbonate; caesium carbonate; In methanol; diethyl ether; water;
DOI:10.1055/s-0031-1290444