diethyl 1-(benzyloxycarbonylamino)-1-trifluoromethylbut-3-yne-1-ylphosphonate

Base Information

Chemical Name:diethyl 1-(benzyloxycarbonylamino)-1-trifluoromethylbut-3-yne-1-ylphosphonate
CAS No.:1228473-25-3
Molecular Formula:C₁₇H₂₁F₃NO₅P
Molecular Weight:407.326
Hs Code.:

Synonyms:diethyl 1-(benzyloxycarbonylamino)-1-trifluoromethylbut-3-yne-1-ylphosphonate

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Chemical Property of diethyl 1-(benzyloxycarbonylamino)-1-trifluoromethylbut-3-yne-1-ylphosphonate

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Technology Process of diethyl 1-(benzyloxycarbonylamino)-1-trifluoromethylbut-3-yne-1-ylphosphonate

There total 2 articles about diethyl 1-(benzyloxycarbonylamino)-1-trifluoromethylbut-3-yne-1-ylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 296238-72-7
diethyl (N-benzyloxycarbonyl-2,2,2-trifluoroethaneimidoyl)phosphonate

: 18295-60-8
allenylmagnesium bromide

: 1228473-25-3
diethyl 1-(benzyloxycarbonylamino)-1-trifluoromethylbut-3-yne-1-ylphosphonate

Guidance literature:: diethyl (N-benzyloxycarbonyl-2,2,2-trifluoroethaneimidoyl)phosphonate; allenylmagnesium bromide; In diethyl ether; at -78 - 20 ℃; for 5h;

With ammonium chloride; In diethyl ether; water;
DOI:10.1016/j.jfluchem.2009.12.003

Reference yield:

: 296238-72-7
diethyl (N-benzyloxycarbonyl-2,2,2-trifluoroethaneimidoyl)phosphonate

: 106-96-7
propargyl bromide

: 1228473-25-3
diethyl 1-(benzyloxycarbonylamino)-1-trifluoromethylbut-3-yne-1-ylphosphonate

Guidance literature:: With magnesium; In diethyl ether; at -78 ℃;
DOI:10.1002/ejoc.202100040

Reference yield: 92.0%

: 1228473-25-3
diethyl 1-(benzyloxycarbonylamino)-1-trifluoromethylbut-3-yne-1-ylphosphonate

: 121177-79-5
1-azido-1H,1H,2H,2H-perfluorodecane

: 1233220-50-2
C₂₇H₂₅F₂₀N₄O₅P

Guidance literature:: With sodium ascorbate; copper(II) sulfate; In water; tert-butyl alcohol; at 80 ℃; for 2h;
DOI:10.1016/j.jfluchem.2009.12.003