Technology Process of 13-<(tetrahydro-2H-pyran-2-yl)-oxy>-2,4-tridecandiyn-1-ol
There total 1 articles about 13-<(tetrahydro-2H-pyran-2-yl)-oxy>-2,4-tridecandiyn-1-ol which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydroxylamine hydrochloride; isopropylamine; copper(l) chloride;
In
methanol;
for 1h;
DOI:10.1016/S0040-4020(01)87295-1
- Guidance literature:
-
Multi-step reaction with 9 steps
1: LAH / diethyl ether / 3 h / Ambient temperature
2: 89 percent / MnO2 / CHCl3 / 5 h / Ambient temperature
3: 1.) Mg / 1.) ether, r.t., 1 h; 2.) THF/ether, r.t., 1 h
4: 85 percent / pyridine / 6 h / Ambient temperature
5: 78 percent / PPTS / ethanol / 2 h / 55 °C
6: 75 percent / pyridinium dichromate / CH2Cl2 / 6 h / Ambient temperature
7: AgNO3, KOH / ethanol; H2O / 2 h / Ambient temperature
8: diethyl ether / 0.5 h / 0 °C
9: 89 percent / H2, quinoline / Pd-CaCO3 / hexane
With
pyridine; quinoline; manganese(IV) oxide; potassium hydroxide; lithium aluminium tetrahydride; dipyridinium dichromate; hydrogen; pyridinium p-toluenesulfonate; silver nitrate; magnesium;
Lindlar's catalyst;
In
diethyl ether; ethanol; hexane; dichloromethane; chloroform; water;
DOI:10.1016/S0040-4020(01)87295-1
- Guidance literature:
-
Multi-step reaction with 5 steps
1: LAH / diethyl ether / 3 h / Ambient temperature
2: 89 percent / MnO2 / CHCl3 / 5 h / Ambient temperature
3: 1.) Mg / 1.) ether, r.t., 1 h; 2.) THF/ether, r.t., 1 h
4: 85 percent / pyridine / 6 h / Ambient temperature
5: 78 percent / PPTS / ethanol / 2 h / 55 °C
With
pyridine; manganese(IV) oxide; lithium aluminium tetrahydride; pyridinium p-toluenesulfonate; magnesium;
In
diethyl ether; ethanol; chloroform;
DOI:10.1016/S0040-4020(01)87295-1