methyl N-[(Z)-3-{[1-(4-chlorophenyl)pyrazol-3-yl]oxy}-1-methylprop-1-enyl]-N-methoxycarbamate

Base Information

Chemical Name:methyl N-[(Z)-3-{[1-(4-chlorophenyl)pyrazol-3-yl]oxy}-1-methylprop-1-enyl]-N-methoxycarbamate
CAS No.:1445331-11-2
Molecular Formula:C₁₆H₁₈ClN₃O₄
Molecular Weight:351.79
Hs Code.:

Synonyms:methyl N-[(Z)-3-{[1-(4-chlorophenyl)pyrazol-3-yl]oxy}-1-methylprop-1-enyl]-N-methoxycarbamate

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Chemical Property of methyl N-[(Z)-3-{[1-(4-chlorophenyl)pyrazol-3-yl]oxy}-1-methylprop-1-enyl]-N-methoxycarbamate

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Technology Process of methyl N-[(Z)-3-{[1-(4-chlorophenyl)pyrazol-3-yl]oxy}-1-methylprop-1-enyl]-N-methoxycarbamate

There total 5 articles about methyl N-[(Z)-3-{[1-(4-chlorophenyl)pyrazol-3-yl]oxy}-1-methylprop-1-enyl]-N-methoxycarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: methyl N-[(1RS,2SR)-3-{[1-(4-chlorophenyl)pyrazol-3-yl]oxy}-2-hydroxy-1-methylpropyl]-N-methoxycarbamate

: 1445331-11-2
methyl N-[(Z)-3-{[1-(4-chlorophenyl)pyrazol-3-yl]oxy}-1-methylprop-1-enyl]-N-methoxycarbamate

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 0 - 20 ℃; for 25h;

Reference yield:

: methyl N-[3-[1-(4-chlorophenyl)pyrazol-3-yl]oxy-2-hydroxy-1-methyl-propyl]-N-methoxy-carbamate

: 1445331-11-2
methyl N-[(Z)-3-{[1-(4-chlorophenyl)pyrazol-3-yl]oxy}-1-methylprop-1-enyl]-N-methoxycarbamate

Guidance literature:: With azodicarbonic acid diisopropyl ester; triphenylphosphine; In tetrahydrofuran; at -15 - 20 ℃; for 25h;

Reference yield:

: (±)-1-(4-chlorophenyl)-3-[[(2R,3S)-3-methyloxiran-2-yl]methoxy]pyrazole

: 1445331-11-2
methyl N-[(Z)-3-{[1-(4-chlorophenyl)pyrazol-3-yl]oxy}-1-methylprop-1-enyl]-N-methoxycarbamate

Guidance literature:: Multi-step reaction with 4 steps

1: potassium tert-butylate / dimethyl sulfoxide / 20 h / 90 °C

2: sodium ethanolate / ethanol

3: sodium hydrogencarbonate / tetrahydrofuran / 20 °C

4: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 25 h / 0 - 20 °C

With di-isopropyl azodicarboxylate; potassium tert-butylate; sodium ethanolate; sodium hydrogencarbonate; triphenylphosphine; In tetrahydrofuran; ethanol; dimethyl sulfoxide;