C₄₅H₄₇N₃O₉

Base Information

Chemical Name:C₄₅H₄₇N₃O₉
CAS No.:947747-44-6
Molecular Formula:C₄₅H₄₇N₃O₉
Molecular Weight:773.883
Hs Code.:

C<sub>45</sub>H<sub>47</sub>N<sub>3</sub>O<sub>9</sub>

Synonyms:C₄₅H₄₇N₃O₉

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Chemical Property of C₄₅H₄₇N₃O₉

Chemical Property:

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Technology Process of C₄₅H₄₇N₃O₉

There total 12 articles about C₄₅H₄₇N₃O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 947747-43-5
(2S,3S)-3-azido-2-benzyloxy-4-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyloxy)butanal

: 947747-44-6
C₄₅H₄₇N₃O₉

Guidance literature:: With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; In water; tert-butyl alcohol;
DOI:10.1016/j.tetlet.2007.05.161

Reference yield:

: 947747-35-5
C₄₃H₄₂O₇S

: 947747-44-6
C₄₅H₄₇N₃O₉

Guidance literature:: Multi-step reaction with 6 steps

1: 94 percent / NaN₃ / dimethylformamide

2: 86 percent / PPTs / methanol

3: 64 percent / MeOTf / CH₂Cl₂

4: 81 percent / DDQ / CH₂Cl₂; methanol

5: 91 percent / TPAP; NMO; MS₄A / acetonitrile

6: 85 percent / NaClO₂; NaH₂PO₄; 2-methyl-2-butene / 2-methyl-propan-2-ol; H₂O

With sodium chlorite; sodium dihydrogenphosphate; sodium azide; N-methyl-2-indolinone; tetrapropylammonium perruthennate; 2-methyl-but-2-ene; pyridinium p-toluenesulfonate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; methyl trifluoromethanesulfonate; In methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol;
DOI:10.1016/j.tetlet.2007.05.161

Reference yield:

: 947747-20-8
C₄₂H₄₀O₅

: 947747-44-6
C₄₅H₄₇N₃O₉

Guidance literature:: Multi-step reaction with 7 steps

1: 88 percent / pyridine

2: 94 percent / NaN₃ / dimethylformamide

3: 86 percent / PPTs / methanol

4: 64 percent / MeOTf / CH₂Cl₂

5: 81 percent / DDQ / CH₂Cl₂; methanol

6: 91 percent / TPAP; NMO; MS₄A / acetonitrile

7: 85 percent / NaClO₂; NaH₂PO₄; 2-methyl-2-butene / 2-methyl-propan-2-ol; H₂O

With sodium chlorite; sodium dihydrogenphosphate; sodium azide; N-methyl-2-indolinone; tetrapropylammonium perruthennate; 2-methyl-but-2-ene; pyridinium p-toluenesulfonate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; methyl trifluoromethanesulfonate; In pyridine; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol;
DOI:10.1016/j.tetlet.2007.05.161