methyl 4-{[2-azido-2-deoxy-4,6-O-(4-methoxybenzylidene)-α-D-galactopyranosyl]sulfanyl}butyrate

Base Information

• Chemical Name: methyl 4-{[2-azido-2-deoxy-4,6-O-(4-methoxybenzylidene)-α-D-galactopyranosyl]sulfanyl}butyrate
• CAS No.: 1040380-10-6
• Molecular Formula: C₁₉H₂₅N₃O₇S
• Molecular Weight: 439.489

Synonyms:methyl 4-{[2-azido-2-deoxy-4,6-O-(4-methoxybenzylidene)-α-D-galactopyranosyl]sulfanyl}butyrate

Chemical Property of methyl 4-{[2-azido-2-deoxy-4,6-O-(4-methoxybenzylidene)-α-D-galactopyranosyl]sulfanyl}butyrate

Chemical Property:

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Technology Process of methyl 4-{[2-azido-2-deoxy-4,6-O-(4-methoxybenzylidene)-α-D-galactopyranosyl]sulfanyl}butyrate

There total 1 articles about methyl 4-{[2-azido-2-deoxy-4,6-O-(4-methoxybenzylidene)-α-D-galactopyranosyl]sulfanyl}butyrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

C11H19N3O6S + p-Anisaldehyde dimethyl acetal (2186-92-7) → methyl 4-{[2-azido-2-deoxy-4,6-O-(4-methoxybenzylidene)-α-D-galactopyranosyl]sulfanyl}butyrate (1040380-10-6) + methyl 4-{[2-azido-2-deoxy-4,6-O-(4-methoxybenzylidene)-β-D-galactopyranosyl]sulfanyl}butyrate (1040380-12-8)

Guidance literature:

With toluene-4-sulfonic acid; In N,N-dimethyl-formamide; at 50 ℃; for 1h; under 15.0015 - 22.5023 Torr;

DOI:10.1055/s-2008-1066982

Reference yield: 99.0%

methyl 4-{[2-azido-2-deoxy-4,6-O-(4-methoxybenzylidene)-α-D-galactopyranosyl]sulfanyl}butyrate (1040380-10-6) + t-butyldimethylsiyl triflate (69739-34-0) → methyl 4-{[2-azido-3-O-(tert-butyldimethylsilyl)-2-deoxy-4,6-O-(4-methoxybenzylidene)-α-D-galactopyranosyl]sulfanyl}butyrate (1040380-14-0)

Guidance literature:

With pyridine; In N,N-dimethyl-formamide; at 0 ℃; for 0.333333h;

DOI:10.1055/s-2008-1066982

upstream raw materials:

p-Anisaldehyde dimethyl acetal

Downstream raw materials:

methyl 4-{[2-azido-3-O-(tert-butyldimethylsilyl)-2-deoxy-4,6-O-(4-methoxybenzylidene)-α-D-galactopyranosyl]sulfanyl}butyrate

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