4-(5'-(4''-methyl-1'',4''-diazepan-1''-yl)benzimidazol-2'-yl)-2-nitroaniline

Base Information

Chemical Name:4-(5'-(4''-methyl-1'',4''-diazepan-1''-yl)benzimidazol-2'-yl)-2-nitroaniline
CAS No.:1339046-00-2
Molecular Formula:C₁₉H₂₂N₆O₂
Molecular Weight:366.423
Hs Code.:

Synonyms:4-(5'-(4''-methyl-1'',4''-diazepan-1''-yl)benzimidazol-2'-yl)-2-nitroaniline

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Chemical Property of 4-(5'-(4''-methyl-1'',4''-diazepan-1''-yl)benzimidazol-2'-yl)-2-nitroaniline

Chemical Property:

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Technology Process of 4-(5'-(4''-methyl-1'',4''-diazepan-1''-yl)benzimidazol-2'-yl)-2-nitroaniline

There total 4 articles about 4-(5'-(4''-methyl-1'',4''-diazepan-1''-yl)benzimidazol-2'-yl)-2-nitroaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4318-37-0
1-Methylhomopiperazine

: 1339046-00-2
4-(5'-(4''-methyl-1'',4''-diazepan-1''-yl)benzimidazol-2'-yl)-2-nitroaniline

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / ISOPROPYLAMIDE / 125 °C / Inert atmosphere

2.1: hydrogen / 5%-palladium/activated carbon / ethyl acetate; methanol / 20 °C

3.1: acetic acid / ethanol / 48 h / Reflux; Inert atmosphere

3.2: pH 12

With hydrogen; potassium carbonate; acetic acid; 5%-palladium/activated carbon; In methanol; ethanol; ISOPROPYLAMIDE; ethyl acetate;

Reference yield:

: 1253838-90-2
4-(4-methyl-1,4-diazepan-1-yl)benzene-1,2-diamine

: ethyl 4-amino-3-nitrobenzimidate hydrochloride

: 1339046-00-2
4-(5'-(4''-methyl-1'',4''-diazepan-1''-yl)benzimidazol-2'-yl)-2-nitroaniline

Guidance literature:: 4-(4-methyl-1,4-diazepan-1-yl)benzene-1,2-diamine; ethyl 4-amino-3-nitrobenzimidate hydrochloride; With acetic acid; In ethanol; for 48h; Reflux; Inert atmosphere;

With ammonia; In water; pH=12;

Reference yield:

: 1635-61-6
5-chloro-2-nitroaniline

: 1339046-00-2
4-(5'-(4''-methyl-1'',4''-diazepan-1''-yl)benzimidazol-2'-yl)-2-nitroaniline

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / ISOPROPYLAMIDE / 125 °C / Inert atmosphere

2.1: hydrogen / 5%-palladium/activated carbon / ethyl acetate; methanol / 20 °C

3.1: acetic acid / ethanol / 48 h / Reflux; Inert atmosphere

3.2: pH 12

With hydrogen; potassium carbonate; acetic acid; 5%-palladium/activated carbon; In methanol; ethanol; ISOPROPYLAMIDE; ethyl acetate;