2-(methoxycarbonyl)phenyl 3-O-(prop-2-enyl)-1-thio-β-D-galactopyranoside

Base Information

Chemical Name:2-(methoxycarbonyl)phenyl 3-O-(prop-2-enyl)-1-thio-β-D-galactopyranoside
CAS No.:1312289-96-5
Molecular Formula:C₁₇H₂₂O₇S
Molecular Weight:370.423
Hs Code.:

Synonyms:2-(methoxycarbonyl)phenyl 3-O-(prop-2-enyl)-1-thio-β-D-galactopyranoside

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Chemical Property of 2-(methoxycarbonyl)phenyl 3-O-(prop-2-enyl)-1-thio-β-D-galactopyranoside

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Technology Process of 2-(methoxycarbonyl)phenyl 3-O-(prop-2-enyl)-1-thio-β-D-galactopyranoside

There total 3 articles about 2-(methoxycarbonyl)phenyl 3-O-(prop-2-enyl)-1-thio-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 106-95-6
allyl bromide

: 382141-84-6
2-(methoxycarbonyl)phenyl 1-thio-β-D-galactopyranoside

: 1312289-96-5
2-(methoxycarbonyl)phenyl 3-O-(prop-2-enyl)-1-thio-β-D-galactopyranoside

Guidance literature:: 2-(methoxycarbonyl)phenyl 1-thio-β-D-galactopyranoside; With di(n-butyl)tin oxide; In methanol; for 28h; Inert atmosphere; Reflux;

allyl bromide; With tetra-(n-butyl)ammonium iodide; In tetrahydrofuran; for 3h; Inert atmosphere; Reflux;
DOI:10.1016/j.bmc.2011.03.022

Reference yield:

: 25878-60-8
D-galactose pentaacetate

: 1312289-96-5
2-(methoxycarbonyl)phenyl 3-O-(prop-2-enyl)-1-thio-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: boron trifluoride diethyl etherate / dichloromethane / 17 h / 20 °C / Inert atmosphere

2.1: methanol; sodium methylate / 20 °C / Inert atmosphere

3.1: di(n-butyl)tin oxide / methanol / 28 h / Inert atmosphere; Reflux

3.2: 3 h / Inert atmosphere; Reflux

With methanol; boron trifluoride diethyl etherate; sodium methylate; di(n-butyl)tin oxide; In methanol; dichloromethane;
DOI:10.1016/j.bmc.2011.03.022

Reference yield:

: 4892-02-8
Methyl thiosalicylate

: 1312289-96-5
2-(methoxycarbonyl)phenyl 3-O-(prop-2-enyl)-1-thio-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: boron trifluoride diethyl etherate / dichloromethane / 17 h / 20 °C / Inert atmosphere

2.1: methanol; sodium methylate / 20 °C / Inert atmosphere

3.1: di(n-butyl)tin oxide / methanol / 28 h / Inert atmosphere; Reflux

3.2: 3 h / Inert atmosphere; Reflux

With methanol; boron trifluoride diethyl etherate; sodium methylate; di(n-butyl)tin oxide; In methanol; dichloromethane;
DOI:10.1016/j.bmc.2011.03.022