2-(2-azido-3,4,6-tri-O-benzyl-2-deoxy-α-D-mannopyranosyl)ethyl aldehyde

Base Information

Chemical Name:2-(2-azido-3,4,6-tri-O-benzyl-2-deoxy-α-D-mannopyranosyl)ethyl aldehyde
CAS No.:618387-40-9
Molecular Formula:C₂₉H₃₁N₃O₅
Molecular Weight:501.582
Hs Code.:

Synonyms:2-(2-azido-3,4,6-tri-O-benzyl-2-deoxy-α-D-mannopyranosyl)ethyl aldehyde

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Chemical Property of 2-(2-azido-3,4,6-tri-O-benzyl-2-deoxy-α-D-mannopyranosyl)ethyl aldehyde

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Technology Process of 2-(2-azido-3,4,6-tri-O-benzyl-2-deoxy-α-D-mannopyranosyl)ethyl aldehyde

There total 4 articles about 2-(2-azido-3,4,6-tri-O-benzyl-2-deoxy-α-D-mannopyranosyl)ethyl aldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 184290-85-5
3-(2-azido-3,4,6-tri-O-benzyl-2-deoxy-α-D-mannopyranosyl)-propene

: 618387-40-9
2-(2-azido-3,4,6-tri-O-benzyl-2-deoxy-α-D-mannopyranosyl)ethyl aldehyde

Guidance literature:: 3-(2-azido-3,4,6-tri-O-benzyl-2-deoxy-α-D-mannopyranosyl)-propene; With ozone; In dichloromethane; at -78 ℃;

With acetic acid; zinc; at 20 ℃;
DOI:10.1021/jo034446k

Reference yield:

: 157903-84-9
3-(3,4,6-tri-O-benzyl-α-D-glucopyranosyl)-1-propene

: 618387-40-9
2-(2-azido-3,4,6-tri-O-benzyl-2-deoxy-α-D-mannopyranosyl)ethyl aldehyde

Guidance literature:: Multi-step reaction with 3 steps

1.1: pyridine / CH₂Cl₂ / 1 h / 0 °C

2.1: 120 mg / NaN₃ / dimethylformamide / 144 h / 70 °C

3.1: O₃ / CH₂Cl₂ / -78 °C

3.2: Zn; HOAc / 20 °C

With pyridine; sodium azide; ozone; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo034446k

Reference yield:

: 192929-44-5
Trifluoro-methanesulfonic acid (2R,3S,4S,5R,6R)-2-allyl-4,5-bis-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-3-yl ester

: 618387-40-9
2-(2-azido-3,4,6-tri-O-benzyl-2-deoxy-α-D-mannopyranosyl)ethyl aldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: 120 mg / NaN₃ / dimethylformamide / 144 h / 70 °C

2.1: O₃ / CH₂Cl₂ / -78 °C

2.2: Zn; HOAc / 20 °C

With sodium azide; ozone; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo034446k