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C66H78O15

Base Information
  • Chemical Name:C66H78O15
  • CAS No.:1375576-66-1
  • Molecular Formula:C66H78O15
  • Molecular Weight:1111.34
  • Hs Code.:
C<sub>66</sub>H<sub>78</sub>O<sub>15</sub>

Synonyms:C66H78O15

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Chemical Property of C66H78O15
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Technology Process of C66H78O15

There total 5 articles about C66H78O15 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 ℃; for 2h; Inert atmosphere; Molecular sieve;
DOI:10.1016/j.ejmech.2012.02.043
Guidance literature:
Multi-step reaction with 3 steps
1.1: pyridine; osmium(VIII) oxide / diethyl ether / -70 - 20 °C
2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 3 h / -60 °C
2.2: -60 - 20 °C
3.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 2 h / 0 °C / Inert atmosphere; Molecular sieve
With pyridine; osmium(VIII) oxide; oxalyl dichloride; trimethylsilyl trifluoromethanesulfonate; dimethyl sulfoxide; In diethyl ether; dichloromethane; 2.1: Swern oxidation / 2.2: Swern oxidation;
DOI:10.1016/j.ejmech.2012.02.043
Guidance literature:
Multi-step reaction with 2 steps
1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 3 h / -60 °C
1.2: -60 - 20 °C
2.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 2 h / 0 °C / Inert atmosphere; Molecular sieve
With oxalyl dichloride; trimethylsilyl trifluoromethanesulfonate; dimethyl sulfoxide; In dichloromethane; 1.1: Swern oxidation / 1.2: Swern oxidation;
DOI:10.1016/j.ejmech.2012.02.043
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