5-(2-Aminomethyl-3,5-dimethoxy-phenoxy)-pentanoic acid; compound with acetic acid

Base Information

Chemical Name:5-(2-Aminomethyl-3,5-dimethoxy-phenoxy)-pentanoic acid; compound with acetic acid
CAS No.:125666-73-1
Molecular Formula:C₂H₄O₂*C₁₄H₂₁NO₅
Molecular Weight:343.377
Hs Code.:

Synonyms:5-(2-Aminomethyl-3,5-dimethoxy-phenoxy)-pentanoic acid; compound with acetic acid

Suppliers and Price of 5-(2-Aminomethyl-3,5-dimethoxy-phenoxy)-pentanoic acid; compound with acetic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 5-(2-Aminomethyl-3,5-dimethoxy-phenoxy)-pentanoic acid; compound with acetic acid

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 5-(2-Aminomethyl-3,5-dimethoxy-phenoxy)-pentanoic acid; compound with acetic acid

There total 5 articles about 5-(2-Aminomethyl-3,5-dimethoxy-phenoxy)-pentanoic acid; compound with acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 115109-62-1
5-(2-hydroximinomethyl-3,5-dimethoxyphenoxy)valeric acid

: 125666-73-1
5-(2-Aminomethyl-3,5-dimethoxy-phenoxy)-pentanoic acid; compound with acetic acid

Guidance literature:: With hydrogen; palladium on activated charcoal; In acetic acid; at 25 ℃; for 2h; under 2280 Torr;
DOI:10.1021/jo00299a011

Reference yield:

: 500-99-2
3,5-dimethoxyphenol

: 125666-73-1
5-(2-Aminomethyl-3,5-dimethoxy-phenoxy)-pentanoic acid; compound with acetic acid

Guidance literature:: Multi-step reaction with 4 steps

1: POCl₃ / 15 h / 25 °C

2: 1.) K₂CO₃, 2.) 2N aq. NaOH / 1.) 3-methyl-2-butanone, reflux, 21h, 2.) 30 min

3: 86 percent / NH₂OH, Na₂CO₃ / H₂O / 2 h

4: H₂ / 10percent Pd/C / aq. acetic acid / 2 h / 25 °C / 2280 Torr

With sodium hydroxide; hydrogen; hydroxylamine; sodium carbonate; potassium carbonate; trichlorophosphate; palladium on activated charcoal; In water; acetic acid;
DOI:10.1021/jo00299a011

Reference yield:

: 708-76-9
2-hydroxy-4,6-dimethoxybenzaldehyde

: 125666-73-1
5-(2-Aminomethyl-3,5-dimethoxy-phenoxy)-pentanoic acid; compound with acetic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) K₂CO₃, 2.) 2N aq. NaOH / 1.) 3-methyl-2-butanone, reflux, 21h, 2.) 30 min

2: 86 percent / NH₂OH, Na₂CO₃ / H₂O / 2 h

3: H₂ / 10percent Pd/C / aq. acetic acid / 2 h / 25 °C / 2280 Torr

With sodium hydroxide; hydrogen; hydroxylamine; sodium carbonate; potassium carbonate; palladium on activated charcoal; In water; acetic acid;
DOI:10.1021/jo00299a011