N-[4-(4-Bromo-butoxy)-phenyl]-N'-(4-dodecyloxy-phenyl)-diazene N'-oxide

Base Information

Chemical Name:N-[4-(4-Bromo-butoxy)-phenyl]-N'-(4-dodecyloxy-phenyl)-diazene N'-oxide
CAS No.:78435-35-5
Molecular Formula:C₂₈H₄₁BrN₂O₃
Molecular Weight:533.549
Hs Code.:

Synonyms:N-[4-(4-Bromo-butoxy)-phenyl]-N'-(4-dodecyloxy-phenyl)-diazene N'-oxide

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Chemical Property of N-[4-(4-Bromo-butoxy)-phenyl]-N'-(4-dodecyloxy-phenyl)-diazene N'-oxide

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Technology Process of N-[4-(4-Bromo-butoxy)-phenyl]-N'-(4-dodecyloxy-phenyl)-diazene N'-oxide

There total 4 articles about N-[4-(4-Bromo-butoxy)-phenyl]-N'-(4-dodecyloxy-phenyl)-diazene N'-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 78435-34-4
p-(ω-bromobutoxy)-p'-(dodecyloxy)azobenzene

: 78435-35-5
N-[4-(4-Bromo-butoxy)-phenyl]-N'-(4-dodecyloxy-phenyl)-diazene N'-oxide

Guidance literature:: With dihydrogen peroxide; In acetic acid; at 65 ℃; for 48h;
DOI:10.1021/ja00408a021

Reference yield:

: 65039-19-2
4-(dodecyloxy)aniline

: 78435-35-5
N-[4-(4-Bromo-butoxy)-phenyl]-N'-(4-dodecyloxy-phenyl)-diazene N'-oxide

Guidance literature:: Multi-step reaction with 4 steps

1: NaNO₂, HCl

4: 56 percent / 30percent aq. H₂O₂ / acetic acid / 48 h / 65 °C

With hydrogenchloride; dihydrogen peroxide; sodium nitrite; In acetic acid;
DOI:10.1021/ja00408a021

Reference yield:

: 87102-54-3
4-<(4-(dodecyloxy)phenyl)azo>phenol

: 78435-35-5
N-[4-(4-Bromo-butoxy)-phenyl]-N'-(4-dodecyloxy-phenyl)-diazene N'-oxide

Guidance literature:: Multi-step reaction with 2 steps

2: 56 percent / 30percent aq. H₂O₂ / acetic acid / 48 h / 65 °C

With dihydrogen peroxide; In acetic acid;
DOI:10.1021/ja00408a021